p-tolylbis(trimethylsilyl)antimony

Base Information

Chemical Name:p-tolylbis(trimethylsilyl)antimony
CAS No.:158502-88-6
Molecular Formula:C₁₃H₂₅SbSi₂
Molecular Weight:359.262
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-tolylbis(trimethylsilyl)antimony

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Technology Process of p-tolylbis(trimethylsilyl)antimony

There total 1 articles about p-tolylbis(trimethylsilyl)antimony which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 75-77-4
chloro-trimethyl-silane

: 87856-09-5
dichloro(4-methylphenyl)stibine

: 158502-88-6
p-tolylbis(trimethylsilyl)antimony

Guidance literature:: With Mg; In tetrahydrofuran; byproducts: MgCl2; Ar atmosphere, addn. of soln. of Sb compound to mixture of Mg and Me3SiCl in THF, stirring (room temp., 12 h); removement of solvent , extn. (petroleum ether), filtration, evapn. of solvent; elem. anal.;

Reference yield: 26.0%

: 158502-88-6
p-tolylbis(trimethylsilyl)antimony

: CH₃C₆H₄Sb

Guidance literature:: With air; In toluene; byproducts: ((CH3)3Si)2O; oxidn. of p-TolSb(SiMe3)2 in toluene by a very slow eccess of air over several d;

Reference yield: 26.0%

: 158502-88-6
p-tolylbis(trimethylsilyl)antimony

: 445401-73-0
bis(di-p-tolylantimony)oxide

: (C₆H₄CH₃)2SbOSi(CH₃)3

: [p-tolylantimony]n

: 445401-71-8
tetra-p-tolyldistibane

: 5395-43-7
tri(p-tolyl)antimony

Guidance literature:: With O₂; In tetrahydrofuran; byproducts: ((CH3)3Si)2O; several days in air; other solvent: toluene, mesitylene, 1,4-dioxane andDMF; separation of crystals, washing (petroleum ether); elem. anal.;