2-(3,4-dibenzyloxybenzoyloxy) 4,5,6-trimethoxy acetophenone

Base Information

Chemical Name:2-(3,4-dibenzyloxybenzoyloxy) 4,5,6-trimethoxy acetophenone
CAS No.:55274-36-7
Molecular Formula:C₃₂H₃₀O₈
Molecular Weight:542.585
Hs Code.:

Synonyms:2-(3,4-dibenzyloxybenzoyloxy) 4,5,6-trimethoxy acetophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3,4-dibenzyloxybenzoyloxy) 4,5,6-trimethoxy acetophenone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(3,4-dibenzyloxybenzoyloxy) 4,5,6-trimethoxy acetophenone

There total 2 articles about 2-(3,4-dibenzyloxybenzoyloxy) 4,5,6-trimethoxy acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6962-57-8
3,6-dihydroxy-2,4-dimethoxyacetophenone

: 55274-36-7
2-(3,4-dibenzyloxybenzoyloxy) 4,5,6-trimethoxy acetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / Heating

2: pyridine / 3 h / 120 °C

With pyridine; potassium carbonate; In acetone;
DOI:10.1021/jm00161a021

Reference yield:

: 55274-36-7
2-(3,4-dibenzyloxybenzoyloxy) 4,5,6-trimethoxy acetophenone

Guidance literature:: 2-Hydroxy-4,5,6-trimethoxyacetophenon VI, 3,4-Dibenzyloxy-benzoylchlorid, Py;

Reference yield:

: 55274-36-7
2-(3,4-dibenzyloxybenzoyloxy) 4,5,6-trimethoxy acetophenone

: 34334-69-5
cirsiliol

Guidance literature:: Multi-step reaction with 6 steps

1: KOH, pyridine / 4 h / 60 °C

2: 88 percent / AcONa, AcOH / 3 h / 140 - 145 °C

3: 97 percent / H₂ / 10percent Pd/C / methanol; ethyl acetate

4: pyridine / Heating

5: AlCl₃ / acetonitrile / 1.5 h / 60 °C

6: 6 M HCl / methanol / 4 h / Heating

With pyridine; hydrogenchloride; potassium hydroxide; aluminium trichloride; hydrogen; sodium acetate; acetic acid; palladium on activated charcoal; In methanol; ethyl acetate; acetonitrile;
DOI:10.1021/jm00161a021