tert-butyl [4-(3,5-bis-n-perfluorobutylbenzyl)-2-methylphenyl]-carbamate

Base Information

Chemical Name:tert-butyl [4-(3,5-bis-n-perfluorobutylbenzyl)-2-methylphenyl]-carbamate
CAS No.:916975-25-2
Molecular Formula:C₂₇H₂₁F₁₈NO₂
Molecular Weight:733.44
Hs Code.:

Synonyms:tert-butyl [4-(3,5-bis-n-perfluorobutylbenzyl)-2-methylphenyl]-carbamate

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Chemical Property of tert-butyl [4-(3,5-bis-n-perfluorobutylbenzyl)-2-methylphenyl]-carbamate

Chemical Property:

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Technology Process of tert-butyl [4-(3,5-bis-n-perfluorobutylbenzyl)-2-methylphenyl]-carbamate

There total 5 articles about tert-butyl [4-(3,5-bis-n-perfluorobutylbenzyl)-2-methylphenyl]-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 508223-54-9
[2-methyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]carbamic acid tert-butyl ester

: 916975-24-1
3,5-bis-n-perfluorobutylbenzyl bromide

: 916975-25-2
tert-butyl [4-(3,5-bis-n-perfluorobutylbenzyl)-2-methylphenyl]-carbamate

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 85 ℃; for 2h;

Reference yield:

: 916975-23-0
[3,5-bis(perfluorobutyl)] phenylmethanol

: 916975-25-2
tert-butyl [4-(3,5-bis-n-perfluorobutylbenzyl)-2-methylphenyl]-carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide; triphenylphosphine / dichloromethane / 10 h / 20 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 2 h / 85 °C

With carbon tetrabromide; sodium carbonate; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; dichloromethane; water;

Reference yield:

: 916975-22-9
methyl 3,5-bis-n-butylbenzoate

: 916975-25-2
tert-butyl [4-(3,5-bis-n-perfluorobutylbenzyl)-2-methylphenyl]-carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

1.2: 0.5 h

2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 10 h / 20 °C

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 2 h / 85 °C

With lithium aluminium tetrahydride; carbon tetrabromide; sodium carbonate; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;