(Z)-tert-butyl 5-phenyl-3-(((trifluoromethyl)sulfonyl)oxy)pent-2-enoate

Base Information

Chemical Name:(Z)-tert-butyl 5-phenyl-3-(((trifluoromethyl)sulfonyl)oxy)pent-2-enoate
CAS No.:1313532-91-0
Molecular Formula:C₁₆H₁₉F₃O₅S
Molecular Weight:380.385
Hs Code.:

Synonyms:(Z)-tert-butyl 5-phenyl-3-(((trifluoromethyl)sulfonyl)oxy)pent-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-tert-butyl 5-phenyl-3-(((trifluoromethyl)sulfonyl)oxy)pent-2-enoate

Chemical Property:

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Technology Process of (Z)-tert-butyl 5-phenyl-3-(((trifluoromethyl)sulfonyl)oxy)pent-2-enoate

There total 1 articles about (Z)-tert-butyl 5-phenyl-3-(((trifluoromethyl)sulfonyl)oxy)pent-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 95679-57-5
tert-butyl 5-phenyl-3-oxopentanoate

: 1313532-91-0
(Z)-tert-butyl 5-phenyl-3-(((trifluoromethyl)sulfonyl)oxy)pent-2-enoate

Guidance literature:: tert-butyl 5-phenyl-3-oxopentanoate; With lithium hydroxide; In water; toluene; at 10 ℃; for 0.0833333h;

trifluoromethylsulfonic anhydride; In water; toluene; at 25 ℃;
DOI:10.1021/jo201042c

Reference yield: 93.0%

: 1313532-91-0
(Z)-tert-butyl 5-phenyl-3-(((trifluoromethyl)sulfonyl)oxy)pent-2-enoate

: tert-butyl 5-phenylpent-2-ynoate

Guidance literature:: With tetrabutyl ammonium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;
DOI:10.1248/cpb.c15-00146

Reference yield:

: 623-73-4
diazoacetic acid ethyl ester

: 1313532-91-0
(Z)-tert-butyl 5-phenyl-3-(((trifluoromethyl)sulfonyl)oxy)pent-2-enoate

: 1-(tert-butyl) 5-ethyl (Z)-4-diazo-3-phenethylpent-2-enedioate

Guidance literature:: With 4-methyl-morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo201042c