2-[(1-BENZYL-4-PIPERIDINYL)AMINO]-3-CHLORONAPHTHOQUINONE

Base Information

• Chemical Name: 2-[(1-BENZYL-4-PIPERIDINYL)AMINO]-3-CHLORONAPHTHOQUINONE
• CAS No.: 179115-41-4
• Molecular Formula: C₂₂H₂₁ClN₂O₂
• Molecular Weight: 380.874
• Mol file: 179115-41-4.mol

Synonyms:2-((1-benzylpiperidin-4-yl)amino)-3-chloronaphthalene-1,4-dione

Chemical Property of 2-[(1-BENZYL-4-PIPERIDINYL)AMINO]-3-CHLORONAPHTHOQUINONE

Chemical Property:

Purity/Quality:

95%-98% ^*data from raw suppliers

2-[(1-Benzyl-4-piperidinyl)amino]-3-chloronaphthoquinone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 2-[(1-BENZYL-4-PIPERIDINYL)AMINO]-3-CHLORONAPHTHOQUINONE

There total 5 articles about 2-[(1-BENZYL-4-PIPERIDINYL)AMINO]-3-CHLORONAPHTHOQUINONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

2,3-Dichloro-1,4-naphthoquinone (117-80-6) + 4-amino-1-benzylpiperidine (50541-93-0) → 2-((1-benzylpiperidin-4-yl)amino)-3-chloronaphthalene-1,4-dione (179115-41-4)

Guidance literature:

With triethylamine; In diethyl ether; at 20 ℃; for 24h;

Reference yield:

piperidin-4-one (41661-47-6) → 2-((1-benzylpiperidin-4-yl)amino)-3-chloronaphthalene-1,4-dione (179115-41-4)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium carbonate / acetonitrile / 2 h / 70 °C

2: sodium cyanoborohydride; ammonium acetate / methanol / Reflux

3: 20 °C

With ammonium acetate; sodium cyanoborohydride; sodium carbonate; In methanol; acetonitrile;

DOI:10.1002/cmdc.202000484

Reference yield:

benzyl chloride (100-44-7) → 2-((1-benzylpiperidin-4-yl)amino)-3-chloronaphthalene-1,4-dione (179115-41-4)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium carbonate / acetonitrile / 2 h / 70 °C

2: sodium cyanoborohydride; ammonium acetate / methanol / Reflux

3: 20 °C

With ammonium acetate; sodium cyanoborohydride; sodium carbonate; In methanol; acetonitrile;

DOI:10.1002/cmdc.202000484

upstream raw materials:

2,3-Dichloro-1,4-naphthoquinone

4-amino-1-benzylpiperidine

piperidin-4-one

benzyl chloride

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