2,6-diacetylpyridine bis-4-phenyl-3-thiosemicarbazone

Base Information

• Chemical Name: 2,6-diacetylpyridine bis-4-phenyl-3-thiosemicarbazone
• CAS No.: 134293-68-8
• Molecular Formula: C₂₃H₂₃N₇S₂
• Molecular Weight: 461.615
• Mol file: 134293-68-8.mol

Synonyms:2,6-diacetylpyridine bis-4-phenyl-3-thiosemicarbazone

Chemical Property of 2,6-diacetylpyridine bis-4-phenyl-3-thiosemicarbazone

Chemical Property:

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Technology Process of 2,6-diacetylpyridine bis-4-phenyl-3-thiosemicarbazone

There total 1 articles about 2,6-diacetylpyridine bis-4-phenyl-3-thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2,6-Diacetylpyridine (1129-30-2) + 4-Phenyl-3-thiosemicarbazide (5351-69-9) → 2,6-diacetylpyridine bis-4-phenyl-3-thiosemicarbazone (134293-68-8)

Guidance literature:

In ethanol; at 20 ℃; for 15h; Reflux;

DOI:10.1002/jccs.201000094

Reference yield: 56.0%

indium(III) chloride + 2,6-diacetylpyridine bis-4-phenyl-3-thiosemicarbazone (134293-68-8) → C46H46Cl2In2N14S4

Guidance literature:

In methanol; ethanol; at 60 ℃; for 6h;

Reference yield: 55.0%

2,6-diacetylpyridine bis-4-phenyl-3-thiosemicarbazone (134293-68-8) + water (7732-18-5) + bis(2,4-pentanedionato)dioxomolybdenum(VI) → C23H21MoN7O2S2*H2O

Guidance literature:

In methanol; for 4h; Reflux;

DOI:10.1134/S002315841802012X

upstream raw materials:

2,6-Diacetylpyridine

4-Phenyl-3-thiosemicarbazide