2-hydroxy-α1,α2-diphenyl-1,3-cyclopentanedimethanol 2,α2-O,O-acetonide α1-O-benzoate

Base Information

Chemical Name:2-hydroxy-α1,α2-diphenyl-1,3-cyclopentanedimethanol 2,α2-O,O-acetonide α1-O-benzoate
CAS No.:1273614-90-6
Molecular Formula:C₂₉H₃₀O₄
Molecular Weight:442.555
Hs Code.:

Synonyms:2-hydroxy-α1,α2-diphenyl-1,3-cyclopentanedimethanol 2,α2-O,O-acetonide α1-O-benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-α1,α2-diphenyl-1,3-cyclopentanedimethanol 2,α2-O,O-acetonide α1-O-benzoate

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Technology Process of 2-hydroxy-α1,α2-diphenyl-1,3-cyclopentanedimethanol 2,α2-O,O-acetonide α1-O-benzoate

There total 1 articles about 2-hydroxy-α1,α2-diphenyl-1,3-cyclopentanedimethanol 2,α2-O,O-acetonide α1-O-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 100-52-7
benzaldehyde

: 120-92-3
cyclopentanone

: 77-76-9
2,2-dimethoxy-propane

: 1273614-90-6
2-hydroxy-α1,α2-diphenyl-1,3-cyclopentanedimethanol 2,α2-O,O-acetonide α1-O-benzoate

: (rel-1S,2S,3R,1αR,2αR)-2-hydroxy-α1,α2-diphenyl-1,3-cyclopentanedimethanol 2,α2-O,O-acetonide α1-O-benzoate

Guidance literature:: benzaldehyde; cyclopentanone; With n-butyllithium; (R)-(+)-3,3'-diphenyl-[1,1'-binaphthalene]-2,2'-diol; In tetrahydrofuran; hexane; at -23 ℃; for 24h;

2,2-dimethoxy-propane; With pyridinium p-toluenesulfonate; In dichloromethane; for 12h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol103156h