tert-butyl {[1-(6-chloro-5-methyl-3-pyridinesulfonyl)-5-phenyl-1H-pyrrol-3-yl]methyl}methylcarbamate

Base Information

Chemical Name:tert-butyl {[1-(6-chloro-5-methyl-3-pyridinesulfonyl)-5-phenyl-1H-pyrrol-3-yl]methyl}methylcarbamate
CAS No.:881678-27-9
Molecular Formula:C₂₃H₂₆ClN₃O₄S
Molecular Weight:475.996
Hs Code.:

Synonyms:tert-butyl {[1-(6-chloro-5-methyl-3-pyridinesulfonyl)-5-phenyl-1H-pyrrol-3-yl]methyl}methylcarbamate

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Chemical Property of tert-butyl {[1-(6-chloro-5-methyl-3-pyridinesulfonyl)-5-phenyl-1H-pyrrol-3-yl]methyl}methylcarbamate

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Technology Process of tert-butyl {[1-(6-chloro-5-methyl-3-pyridinesulfonyl)-5-phenyl-1H-pyrrol-3-yl]methyl}methylcarbamate

There total 3 articles about tert-butyl {[1-(6-chloro-5-methyl-3-pyridinesulfonyl)-5-phenyl-1H-pyrrol-3-yl]methyl}methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 881677-00-5
1-[(6-chloro-5-methylpyridin-3-yl)sulfonyl]-5-phenyl-1H-pyrrole-3-carbaldehyde

: 24424-99-5
di-tert-butyl dicarbonate

: 74-89-5
methylamine

: 881678-27-9
tert-butyl {[1-(6-chloro-5-methyl-3-pyridinesulfonyl)-5-phenyl-1H-pyrrol-3-yl]methyl}methylcarbamate

Guidance literature:: 1-[(6-chloro-5-methylpyridin-3-yl)sulfonyl]-5-phenyl-1H-pyrrole-3-carbaldehyde; methylamine; In tetrahydrofuran; at 20 ℃; for 4h;

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; for 0.05h;

di-tert-butyl dicarbonate; With water; sodium hydrogencarbonate; more than 3 stages;

Reference yield: 77.0%

: 881677-00-5
1-[(6-chloro-5-methylpyridin-3-yl)sulfonyl]-5-phenyl-1H-pyrrole-3-carbaldehyde

: 24424-99-5
di-tert-butyl dicarbonate

: 881678-27-9
tert-butyl {[1-(6-chloro-5-methyl-3-pyridinesulfonyl)-5-phenyl-1H-pyrrol-3-yl]methyl}methylcarbamate

Guidance literature:: 1-[(6-chloro-5-methylpyridin-3-yl)sulfonyl]-5-phenyl-1H-pyrrole-3-carbaldehyde; methylamine; In tetrahydrofuran; at 20 ℃; for 4h;

With methanol; sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃; for 0.05h;

di-tert-butyl dicarbonate; With sodium hydrogencarbonate; In tetrahydrofuran; methanol; water; at 20 ℃; for 0.5h;