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Technology Process of C9H7ClO2

C9H7ClO2

Base Information
  • Chemical Name:C9H7ClO2
  • CAS No.:1401711-45-2
  • Molecular Formula:C9H7ClO2
  • Molecular Weight:182.606
  • Hs Code.:
C<sub>9</sub>H<sub>7</sub>ClO<sub>2</sub>

Synonyms:C9H7ClO2

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Chemical Property of C9H7ClO2
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Technology Process of C9H7ClO2

There total 2 articles about C9H7ClO2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chlorocinnamaldehyde
1794-45-2

2-chlorocinnamaldehyde

C<sub>9</sub>H<sub>7</sub>ClO<sub>2</sub>
1401711-45-2

C9H7ClO2

Guidance literature:
With (S)-2-(diphenyl((triethylsilyl)oxy)methyl)pyrrolidine; dihydrogen peroxide; In dichloromethane; water; at 20 ℃; for 2h; enantioselective reaction;
DOI:10.1039/c3ob00056g

Reference yield:

2-chlorocinnamaldehyde
1794-45-2

2-chlorocinnamaldehyde

C<sub>9</sub>H<sub>7</sub>ClO<sub>2</sub>
1401711-45-2

C9H7ClO2

C<sub>9</sub>H<sub>7</sub>ClO<sub>2</sub>

C9H7ClO2

C<sub>9</sub>H<sub>7</sub>ClO<sub>2</sub>

C9H7ClO2

Guidance literature:
With tert.-butylhydroperoxide; 4-oxalocrotonate tautomerase Q4Y/M45I/F50A mutant; In aq. phosphate buffer; ethanol; at 25 ℃; pH=7.3; stereoselective reaction; Enzymatic reaction;
DOI:10.1002/anie.202001373

Reference yield: 55.0%

methanol
67-56-1

methanol

C<sub>9</sub>H<sub>7</sub>ClO<sub>2</sub>
1401711-45-2

C9H7ClO2

C<sub>10</sub>H<sub>9</sub>ClO<sub>3</sub>
1426928-97-3

C10H9ClO3

Guidance literature:
With N-Bromosuccinimide; sodium carbonate; In dichloromethane; at 20 ℃; for 3h; enantioselective reaction;
DOI:10.1039/c3ob00056g
upstream raw materials:

2-chlorocinnamaldehyde

Downstream raw materials:

C10H9ClO3

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