3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime

Base Information

Chemical Name:3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime
CAS No.:97589-70-3
Molecular Formula:C₅₄H₄₅NO₁₆
Molecular Weight:963.948
Hs Code.:

Synonyms:3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime

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Chemical Property of 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime

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Technology Process of 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime

There total 6 articles about 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 87760-36-9
2,3,6-tri-O-benzoyl-4-O-(2,3,4,5-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol

: 97589-70-3
3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; at 70 ℃; for 20h;
DOI:10.1021/jo00219a017

Reference yield: 76.0%

: 75414-17-4
2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol

: 75414-23-2,97589-70-3,97589-72-5,97589-73-6
C₅₄H₄₅NO₁₆

Guidance literature:: at 70 ℃; for 13h;
DOI:10.1016/S0040-4039(00)92736-9

Reference yield:

: 91280-47-6
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-D-glucopyranose

: 97589-70-3
3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / HBr(gas) / 1,2-dichloro-ethane; acetic acid / 24 h / Ambient temperature

2: 1.) NaI, 2.) diethylamine / 1.) acetone, RT, 15 min, 2.) RT, 16 h

3: 89 percent / hydroxylamine hydrochloride, pyridine / 20 h / 70 °C

With pyridine; hydroxylamine hydrochloride; hydrogen bromide; diethylamine; sodium iodide; In acetic acid; 1,2-dichloro-ethane;
DOI:10.1021/jo00219a017