3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose monohydrate

Base Information

Chemical Name:3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose monohydrate
CAS No.:97523-40-5
Molecular Formula:C₅₄H₄₆O₁₇
Molecular Weight:966.949
Hs Code.:

Synonyms:3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose monohydrate

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Chemical Property of 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose monohydrate

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Technology Process of 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose monohydrate

There total 4 articles about 3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 97589-70-3
3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime

: 97523-40-5
3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose monohydrate

Guidance literature:: With hydrogenchloride; acetaldehyde; In acetonitrile; for 3h; Ambient temperature;
DOI:10.1021/jo00219a017

Reference yield:

: 61198-91-2
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide

: 97523-40-5
3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose monohydrate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaI, 2.) diethylamine / 1.) acetone, RT, 15 min, 2.) RT, 16 h

2: 89 percent / hydroxylamine hydrochloride, pyridine / 20 h / 70 °C

3: 90 percent / acetaldehyde, aq. HCl / acetonitrile / 3 h / Ambient temperature

With pyridine; hydrogenchloride; hydroxylamine hydrochloride; acetaldehyde; diethylamine; sodium iodide; In acetonitrile;
DOI:10.1021/jo00219a017

Reference yield:

: 87760-36-9
2,3,6-tri-O-benzoyl-4-O-(2,3,4,5-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol

: 97523-40-5
3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose monohydrate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / hydroxylamine hydrochloride, pyridine / 20 h / 70 °C

2: 90 percent / acetaldehyde, aq. HCl / acetonitrile / 3 h / Ambient temperature

With pyridine; hydrogenchloride; hydroxylamine hydrochloride; acetaldehyde; In acetonitrile;
DOI:10.1021/jo00219a017