N,N'-bis(2,6-diisopropylphenyl)-5,11-diphenylcoronene-2,3,8,9-tetracarboxdiimide

Base Information

Chemical Name:N,N'-bis(2,6-diisopropylphenyl)-5,11-diphenylcoronene-2,3,8,9-tetracarboxdiimide
CAS No.:1355646-41-1
Molecular Formula:C₆₄H₅₀N₂O₄
Molecular Weight:911.112
Hs Code.:

Synonyms:N,N'-bis(2,6-diisopropylphenyl)-5,11-diphenylcoronene-2,3,8,9-tetracarboxdiimide

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Chemical Property of N,N'-bis(2,6-diisopropylphenyl)-5,11-diphenylcoronene-2,3,8,9-tetracarboxdiimide

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Technology Process of N,N'-bis(2,6-diisopropylphenyl)-5,11-diphenylcoronene-2,3,8,9-tetracarboxdiimide

There total 3 articles about N,N'-bis(2,6-diisopropylphenyl)-5,11-diphenylcoronene-2,3,8,9-tetracarboxdiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.1%

: 14900-39-1
phenylvinylboronic acid

: 331861-94-0
1,7-dibromo-N,N'-bis(2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic acid diimide

: 1355646-46-6
N,N'-bis(2,6-diisopropylphenyl)-5-phenylbenzoperylene-2,3,8,9-tetracarboxdiimides

: 1355646-41-1
N,N'-bis(2,6-diisopropylphenyl)-5,11-diphenylcoronene-2,3,8,9-tetracarboxdiimide

: 82953-57-9
Lumogen F Orange 240

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; benzene; at 80 ℃; for 120h; Inert atmosphere;
DOI:10.1016/j.dyepig.2011.11.009

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1355646-46-6
N,N'-bis(2,6-diisopropylphenyl)-5-phenylbenzoperylene-2,3,8,9-tetracarboxdiimides

: 1355646-41-1
N,N'-bis(2,6-diisopropylphenyl)-5,11-diphenylcoronene-2,3,8,9-tetracarboxdiimide

: 82953-57-9
Lumogen F Orange 240

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; bromine; iodine

2: acetic acid / 1-methyl-pyrrolidin-2-one

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; benzene / 120 h / 80 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; bromine; iodine; sodium carbonate; acetic acid; In 1-methyl-pyrrolidin-2-one; ethanol; water; benzene; 3: Suzuki coupling;
DOI:10.1016/j.dyepig.2011.11.009

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1355646-41-1
N,N'-bis(2,6-diisopropylphenyl)-5,11-diphenylcoronene-2,3,8,9-tetracarboxdiimide

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine; sulfuric acid / 2 h / 20 °C

1.2: 16 h / 80 °C

2.1: acetic acid / 1-methyl-pyrrolidin-2-one / 96 h / 120 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / benzene; water; ethanol / 120 h / 80 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; iodine; sodium carbonate; acetic acid; In 1-methyl-pyrrolidin-2-one; ethanol; water; benzene;