C₂₆H₂₄FNO₅

Base Information

Chemical Name:C₂₆H₂₄FNO₅
CAS No.:1374234-40-8
Molecular Formula:C₂₆H₂₄FNO₅
Molecular Weight:449.479
Hs Code.:

C<sub>26</sub>H<sub>24</sub>FNO<sub>5</sub>

Synonyms:C₂₆H₂₄FNO₅

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Chemical Property of C₂₆H₂₄FNO₅

Chemical Property:

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Technology Process of C₂₆H₂₄FNO₅

There total 6 articles about C₂₆H₂₄FNO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1179986-66-3
ethyl 2-(4-(4-fluorophenoxy)phenyl)-5-isopropoxy-6-nitrobenzofuran-3-carboxylate

: 1374234-40-8
C₂₆H₂₄FNO₅

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethyl acetate; at 20 ℃; for 3h;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1374234-40-8
C₂₆H₂₄FNO₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

2.2: 4 h / 80 °C

3.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

4.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

With potassium phosphate; hydrogen; nitric acid; caesium carbonate; zinc(II) chloride; palladium 10% on activated carbon; palladium diacetate; tert-butyl XPhos; In 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1374234-40-8
C₂₆H₂₄FNO₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / toluene; mineral oil / 2 h / 0 - 20 °C

1.2: Reflux

2.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

3.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

3.2: 4 h / 80 °C

4.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

5.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

6.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

With potassium phosphate; hydrogen; nitric acid; sodium hydride; caesium carbonate; zinc(II) chloride; palladium 10% on activated carbon; palladium diacetate; tert-butyl XPhos; In 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; mineral oil;