toluyl 6-O-tert-butyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-1-thio-Β-D-glucosamine

Base Information

Chemical Name:toluyl 6-O-tert-butyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-1-thio-Β-D-glucosamine
CAS No.:1453169-66-8
Molecular Formula:C₂₂H₃₄Cl₃NO₆SSi
Molecular Weight:575.026
Hs Code.:

Synonyms:toluyl 6-O-tert-butyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-1-thio-Β-D-glucosamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of toluyl 6-O-tert-butyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-1-thio-Β-D-glucosamine

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Technology Process of toluyl 6-O-tert-butyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-1-thio-Β-D-glucosamine

There total 2 articles about toluyl 6-O-tert-butyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-1-thio-Β-D-glucosamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 323195-45-5
p-methylphenyl 2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

: 1453169-66-8
toluyl 6-O-tert-butyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-1-thio-Β-D-glucosamine

Guidance literature:: In 1,2-dichloro-ethane; for 16h; Reflux; Inert atmosphere;
DOI:10.1002/ejoc.201300664

Reference yield:

: 220645-20-5
p-methylphenyl 3,4,6-tri-O-acetyl-2-deoxy-1-thio-2-(2,2,2-trichloroethyloxycarbonylamino)-β-D-glucopyranoside

: 1453169-66-8
toluyl 6-O-tert-butyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-1-thio-Β-D-glucosamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate; methanol

2: pyridine

With pyridine; methanol; sodium methylate;
DOI:10.1021/acschembio.9b00467