2-benzyl-1-[2-(4-trifluoromethyl-phenyl)-allyl]-1,2-dihydro-isoquinoline

Base Information

Chemical Name:2-benzyl-1-[2-(4-trifluoromethyl-phenyl)-allyl]-1,2-dihydro-isoquinoline
CAS No.:862307-03-7
Molecular Formula:C₂₆H₂₂F₃N
Molecular Weight:405.463
Hs Code.:

Synonyms:2-benzyl-1-[2-(4-trifluoromethyl-phenyl)-allyl]-1,2-dihydro-isoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzyl-1-[2-(4-trifluoromethyl-phenyl)-allyl]-1,2-dihydro-isoquinoline

Chemical Property:

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Technology Process of 2-benzyl-1-[2-(4-trifluoromethyl-phenyl)-allyl]-1,2-dihydro-isoquinoline

There total 3 articles about 2-benzyl-1-[2-(4-trifluoromethyl-phenyl)-allyl]-1,2-dihydro-isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 463-49-0
1,2-propanediene

: 455-13-0
4-Iodobenzotrifluoride

: 23277-04-5
2-benzylisoquinolin-2-ium bromide

: 862307-03-7
2-benzyl-1-[2-(4-trifluoromethyl-phenyl)-allyl]-1,2-dihydro-isoquinoline

Guidance literature:: With indium; copper(l) iodide; trifuran-2-yl-phosphane; palladium diacetate; In N,N-dimethyl-formamide; at 40 ℃; for 20h; under 750.06 Torr;
DOI:10.1039/b503213j

Reference yield:

: 119-65-3
isoquinoline

: 862307-03-7
2-benzyl-1-[2-(4-trifluoromethyl-phenyl)-allyl]-1,2-dihydro-isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide / 5 h / 80 °C

2: trifuryl phosphine; In; CuI / Pd(OAc)2 / dimethylformamide / 20 h / 40 °C / 750.06 Torr

With indium; copper(l) iodide; trifuran-2-yl-phosphane; palladium diacetate; In N,N-dimethyl-formamide;
DOI:10.1039/b503213j

Reference yield:

: 100-39-0
benzyl bromide

: 862307-03-7
2-benzyl-1-[2-(4-trifluoromethyl-phenyl)-allyl]-1,2-dihydro-isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide / 5 h / 80 °C

2: trifuryl phosphine; In; CuI / Pd(OAc)2 / dimethylformamide / 20 h / 40 °C / 750.06 Torr

With indium; copper(l) iodide; trifuran-2-yl-phosphane; palladium diacetate; In N,N-dimethyl-formamide;
DOI:10.1039/b503213j