N-<(Phenylmethoxy)carbonyl>glycine 2-bromoethyl ester

Base Information

Chemical Name:N-<(Phenylmethoxy)carbonyl>glycine 2-bromoethyl ester
CAS No.:156539-01-4
Molecular Formula:C₁₂H₁₄BrNO₄
Molecular Weight:316.151
Hs Code.:

Synonyms:N-<(Phenylmethoxy)carbonyl>glycine 2-bromoethyl ester

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Chemical Property of N-<(Phenylmethoxy)carbonyl>glycine 2-bromoethyl ester

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Technology Process of N-<(Phenylmethoxy)carbonyl>glycine 2-bromoethyl ester

There total 1 articles about N-<(Phenylmethoxy)carbonyl>glycine 2-bromoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 540-51-2
2-bromoethanol

: 156539-01-4
N-<(Phenylmethoxy)carbonyl>glycine 2-bromoethyl ester

Guidance literature:: With pyridine; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 16h;
DOI:10.1021/jo00087a053

Reference yield: 86.0%

: 156539-01-4
N-<(Phenylmethoxy)carbonyl>glycine 2-bromoethyl ester

: 156539-07-0
glycine N-<(phenylmethoxy)carbonyl>glycine 2-iodoethyl ester

Guidance literature:: With sodium iodide; In acetone; for 7h; Heating;
DOI:10.1021/jo00087a053

Reference yield:

: 156539-01-4
N-<(Phenylmethoxy)carbonyl>glycine 2-bromoethyl ester

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / NaI / acetone / 7 h / Heating

2: 89 percent / SmI₂ / tetrahydrofuran / 8 h / 40 °C

With samarium diiodide; sodium iodide; In tetrahydrofuran; acetone;
DOI:10.1021/jo00087a053