2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]piperidin-4-ylsulfanyl}phenol

Base Information

Chemical Name:2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]piperidin-4-ylsulfanyl}phenol
CAS No.:1402049-46-0
Molecular Formula:C₃₇H₅₉NO₃S₂
Molecular Weight:630.012
Hs Code.:

Synonyms:2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]piperidin-4-ylsulfanyl}phenol

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Chemical Property of 2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]piperidin-4-ylsulfanyl}phenol

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Technology Process of 2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]piperidin-4-ylsulfanyl}phenol

There total 5 articles about 2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]piperidin-4-ylsulfanyl}phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1402049-45-9
4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)piperidine-1-carboxylic acid ethyl ester

: 1402049-46-0
2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]piperidin-4-ylsulfanyl}phenol

Guidance literature:: 4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)piperidine-1-carboxylic acid ethyl ester; With isopropyl alcohol; potassium hydroxide; at 85 ℃;

pH=6; Acidic aqueous solution;

Reference yield:

: 29976-53-2
N-ethoxycarbonyl-4-piperidone

: 1402049-46-0
2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]piperidin-4-ylsulfanyl}phenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / methanol / 20 h / 45 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 4.5 h / 85 °C

3.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 9 h / 20 °C

4.1: dimethylsulfide borane complex / tetrahydrofuran / 20 °C

5.1: isopropyl alcohol; potassium hydroxide / 85 °C

5.2: pH 6 / Acidic aqueous solution

With hydrogenchloride; lithium hydroxide monohydrate; dimethylsulfide borane complex; water; potassium carbonate; isopropyl alcohol; potassium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 1402049-10-8
4,4-bis-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)piperidine-1-carboxylic acid ethyl ester

: 1402049-46-0
2,6-di-tert-butyl-4-{4-[3,5-di-tert-butyl-4-(4-hydroxybutoxy)phenylsulfanyl]piperidin-4-ylsulfanyl}phenol

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4.5 h / 85 °C

2.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 9 h / 20 °C

3.1: dimethylsulfide borane complex / tetrahydrofuran / 20 °C

4.1: isopropyl alcohol; potassium hydroxide / 85 °C

4.2: pH 6 / Acidic aqueous solution

With lithium hydroxide monohydrate; dimethylsulfide borane complex; water; potassium carbonate; isopropyl alcohol; potassium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;