4-[3,5-di-tert-butyl-4-(3-carboxypropoxy)phenyl-sulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-piperidine-1-carboxylic acid ethyl ester

Base Information

Chemical Name:4-[3,5-di-tert-butyl-4-(3-carboxypropoxy)phenyl-sulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-piperidine-1-carboxylic acid ethyl ester
CAS No.:1402049-44-8
Molecular Formula:C₄₀H₆₁NO₆S₂
Molecular Weight:716.059
Hs Code.:

4-[3,5-di-tert-butyl-4-(3-carboxypropoxy)phenyl-sulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-piperidine-1-carboxylic acid ethyl ester

Synonyms:4-[3,5-di-tert-butyl-4-(3-carboxypropoxy)phenyl-sulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-piperidine-1-carboxylic acid ethyl ester

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Chemical Property of 4-[3,5-di-tert-butyl-4-(3-carboxypropoxy)phenyl-sulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-piperidine-1-carboxylic acid ethyl ester

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Technology Process of 4-[3,5-di-tert-butyl-4-(3-carboxypropoxy)phenyl-sulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-piperidine-1-carboxylic acid ethyl ester

There total 4 articles about 4-[3,5-di-tert-butyl-4-(3-carboxypropoxy)phenyl-sulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-piperidine-1-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: C₄₂H₆₅NO₆S₂

: 1402049-44-8
4-[3,5-di-tert-butyl-4-(3-carboxypropoxy)phenyl-sulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-piperidine-1-carboxylic acid ethyl ester

Guidance literature:: C₄₂H₆₅NO₆S₂; With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 20 ℃; for 9h;

With hydrogenchloride; In tetrahydrofuran; water;

Reference yield:

: 1402049-10-8
4,4-bis-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)piperidine-1-carboxylic acid ethyl ester

: 1402049-44-8
4-[3,5-di-tert-butyl-4-(3-carboxypropoxy)phenyl-sulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-piperidine-1-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4.5 h / 85 °C

2: water; lithium hydroxide monohydrate / tetrahydrofuran / 9 h / 20 °C

With lithium hydroxide monohydrate; water; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 950-59-4
4-hydroxy-3,5-di-tert-butylthiophenol

: 1402049-44-8
4-[3,5-di-tert-butyl-4-(3-carboxypropoxy)phenyl-sulfanyl]-4-(3,5-di-tert-butyl-4-hydroxyphenylsulfanyl)-piperidine-1-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / methanol / 20 h / 45 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4.5 h / 85 °C

3: water; lithium hydroxide monohydrate / tetrahydrofuran / 9 h / 20 °C

With hydrogenchloride; lithium hydroxide monohydrate; water; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;