2-methyl-1-(o-methylbenzyl)-3,4-dihydroisoquinolinium prchlorate

Base Information

Chemical Name:2-methyl-1-(o-methylbenzyl)-3,4-dihydroisoquinolinium prchlorate
CAS No.:116351-59-8
Molecular Formula:C₁₈H₂₀N*ClO₄
Molecular Weight:349.814
Hs Code.:

Synonyms:2-methyl-1-(o-methylbenzyl)-3,4-dihydroisoquinolinium prchlorate

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Chemical Property of 2-methyl-1-(o-methylbenzyl)-3,4-dihydroisoquinolinium prchlorate

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Technology Process of 2-methyl-1-(o-methylbenzyl)-3,4-dihydroisoquinolinium prchlorate

There total 4 articles about 2-methyl-1-(o-methylbenzyl)-3,4-dihydroisoquinolinium prchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 104330-69-0
1-(o-methylbenzyl)-3,4-dihydroisoquinoline

: 74-88-4
methyl iodide

: 116351-59-8
2-methyl-1-(o-methylbenzyl)-3,4-dihydroisoquinolinium prchlorate

Guidance literature:: With silver perchlorate; In acetonitrile; at 25 ℃; for 2h;
DOI:10.1021/jo00256a038

Reference yield:

: 3230-65-7
3,4-dihydroisoquinoline

: 116351-59-8
2-methyl-1-(o-methylbenzyl)-3,4-dihydroisoquinolinium prchlorate

Guidance literature:: Multi-step reaction with 3 steps

1: Mg / 1.) ether, reflux, 1 h, 2.) reflux, 4 h

2: 1.) N-chlorosuccinimide, 2.)KOH / 1.) ether, 25 deg C, 0.5 h, 2.) methanol, 25 deg C, 1 h

3: 67 percent / silver perchlorate / acetonitrile / 2 h / 25 °C

With potassium hydroxide; N-chloro-succinimide; silver perchlorate; magnesium; In acetonitrile;
DOI:10.1021/jo00256a038

Reference yield:

: 552-45-4
1-chloromethyl-2-methylbenzene

: 116351-59-8
2-methyl-1-(o-methylbenzyl)-3,4-dihydroisoquinolinium prchlorate

Guidance literature:: Multi-step reaction with 3 steps

1: Mg / 1.) ether, reflux, 1 h, 2.) reflux, 4 h

2: 1.) N-chlorosuccinimide, 2.)KOH / 1.) ether, 25 deg C, 0.5 h, 2.) methanol, 25 deg C, 1 h

3: 67 percent / silver perchlorate / acetonitrile / 2 h / 25 °C

With potassium hydroxide; N-chloro-succinimide; silver perchlorate; magnesium; In acetonitrile;
DOI:10.1021/jo00256a038