Ethyl 1-[2-(2,4-dichlorophenyl)-2-oxoethyl]-1H-imidazole-2-carboxylate

Base Information

Chemical Name:Ethyl 1-[2-(2,4-dichlorophenyl)-2-oxoethyl]-1H-imidazole-2-carboxylate
CAS No.:1101323-71-0
Molecular Formula:C₁₄H₁₂Cl₂N₂O₃
Molecular Weight:327.167
Hs Code.:

Synonyms:Ethyl 1-[2-(2,4-dichlorophenyl)-2-oxoethyl]-1H-imidazole-2-carboxylate

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Chemical Property of Ethyl 1-[2-(2,4-dichlorophenyl)-2-oxoethyl]-1H-imidazole-2-carboxylate

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Technology Process of Ethyl 1-[2-(2,4-dichlorophenyl)-2-oxoethyl]-1H-imidazole-2-carboxylate

There total 1 articles about Ethyl 1-[2-(2,4-dichlorophenyl)-2-oxoethyl]-1H-imidazole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 33543-78-1
ethyl 1H-imidazole-2-carboxylate

: 2631-72-3
2,4-dichlorophenacyl bromide

: 1101323-71-0
Ethyl 1-[2-(2,4-dichlorophenyl)-2-oxoethyl]-1H-imidazole-2-carboxylate

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 12h;

Reference yield: 82.0%

: 1101323-71-0
Ethyl 1-[2-(2,4-dichlorophenyl)-2-oxoethyl]-1H-imidazole-2-carboxylate

: 168968-73-8
6-(2,4-dichlorophenyl)imidazo[1,2-a]pyrazin-8(7H)-one

Guidance literature:: Ethyl 1-[2-(2,4-dichlorophenyl)-2-oxoethyl]-1H-imidazole-2-carboxylate; With ammonium acetate; acetic acid; for 12h; Reflux;

With sodium carbonate; In water;

Reference yield:

: 1101323-71-0
Ethyl 1-[2-(2,4-dichlorophenyl)-2-oxoethyl]-1H-imidazole-2-carboxylate

: 1101322-32-0
6-[(2-{[6-(2,4-Dichlorophenyl)imidazo[1,2-a]pyrazin-8-yl]amino}ethyl)amino]nicotinonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium acetate; acetic acid / 12 h / Reflux

2.1: trichlorophosphate / 12 h / Reflux

2.2: pH 7

3.1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 12 h / 120 °C

With ammonium acetate; acetic acid; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In dimethyl sulfoxide;