ethyl N-{[(benzyloxy)carbonyl]sulfamoyl}-N-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)glycinate

Base Information

Chemical Name:ethyl N-{[(benzyloxy)carbonyl]sulfamoyl}-N-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)glycinate
CAS No.:1415573-68-0
Molecular Formula:C₂₄H₄₀N₂O₇SSi
Molecular Weight:528.742
Hs Code.:

Synonyms:ethyl N-{[(benzyloxy)carbonyl]sulfamoyl}-N-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)glycinate

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Chemical Property of ethyl N-{[(benzyloxy)carbonyl]sulfamoyl}-N-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)glycinate

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Technology Process of ethyl N-{[(benzyloxy)carbonyl]sulfamoyl}-N-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)glycinate

There total 2 articles about ethyl N-{[(benzyloxy)carbonyl]sulfamoyl}-N-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1189-71-5
isocyanate de chlorosulfonyle

: 1415573-67-9
ethyl N-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)glycinate

: 100-51-6,185532-71-2
benzyl alcohol

: 1415573-68-0
ethyl N-{[(benzyloxy)carbonyl]sulfamoyl}-N-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)glycinate

Guidance literature:: isocyanate de chlorosulfonyle; benzyl alcohol; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

ethyl N-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)glycinate; With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 690992-74-6
trans-4-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}cyclohexanamine

: 1415573-68-0
ethyl N-{[(benzyloxy)carbonyl]sulfamoyl}-N-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)glycinate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / acetonitrile / 1 h / Reflux

2.1: dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: 1 h / 20 °C

With triethylamine; In dichloromethane; acetonitrile;