(S)-N-((R)-1-(3-(cyclopentyloxy)phenyl)ethyl)-2-methylpropane-2-sulfinamide

Base Information

Chemical Name:(S)-N-((R)-1-(3-(cyclopentyloxy)phenyl)ethyl)-2-methylpropane-2-sulfinamide
CAS No.:1309653-53-9
Molecular Formula:C₁₇H₂₇NO₂S
Molecular Weight:309.473
Hs Code.:

Synonyms:(S)-N-((R)-1-(3-(cyclopentyloxy)phenyl)ethyl)-2-methylpropane-2-sulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-((R)-1-(3-(cyclopentyloxy)phenyl)ethyl)-2-methylpropane-2-sulfinamide

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Technology Process of (S)-N-((R)-1-(3-(cyclopentyloxy)phenyl)ethyl)-2-methylpropane-2-sulfinamide

There total 4 articles about (S)-N-((R)-1-(3-(cyclopentyloxy)phenyl)ethyl)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1198223-04-9
(S,E)-N-(3-(cyclopentyloxy)benzylidene)-2-methylpropane-2-sulfinamide

: 75-16-1
methylmagnesium bromide

: 1309653-53-9
(S)-N-((R)-1-(3-(cyclopentyloxy)phenyl)ethyl)-2-methylpropane-2-sulfinamide

Guidance literature:: In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 12h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jm300416h

Reference yield:

: 1309653-52-8
C₁₆H₂₃NO₂S

: 75-16-1
methylmagnesium bromide

: 1309653-53-9
(S)-N-((R)-1-(3-(cyclopentyloxy)phenyl)ethyl)-2-methylpropane-2-sulfinamide

Guidance literature:: C₁₆H₂₃NO₂S; methylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 4h;

With ammonium chloride; In tetrahydrofuran; diethyl ether; water; at 0 ℃; for 0.0833333h;

Reference yield:

: 273722-75-1
3-(cyclopentyloxy)benzaldehyde

: 1309653-53-9
(S)-N-((R)-1-(3-(cyclopentyloxy)phenyl)ethyl)-2-methylpropane-2-sulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1: titanium(IV) isopropylate / toluene / 12 h / 20 - 90 °C / Inert atmosphere

2: tetrahydrofuran; diethyl ether / 12 h / 0 - 20 °C / Inert atmosphere

With titanium(IV) isopropylate; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/jm300416h