2-benzyl-4-tert-butoxycarbonylamino-3-oxo-5-phenyl-pentanoic acid allyl ester

Base Information

Chemical Name:2-benzyl-4-tert-butoxycarbonylamino-3-oxo-5-phenyl-pentanoic acid allyl ester
CAS No.:1027300-21-5
Molecular Formula:C₂₆H₃₁NO₅
Molecular Weight:437.536
Hs Code.:

2-benzyl-4-<i>tert</i>-butoxycarbonylamino-3-oxo-5-phenyl-pentanoic acid allyl ester

Synonyms:2-benzyl-4-tert-butoxycarbonylamino-3-oxo-5-phenyl-pentanoic acid allyl ester

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Chemical Property of 2-benzyl-4-tert-butoxycarbonylamino-3-oxo-5-phenyl-pentanoic acid allyl ester

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Technology Process of 2-benzyl-4-tert-butoxycarbonylamino-3-oxo-5-phenyl-pentanoic acid allyl ester

There total 3 articles about 2-benzyl-4-tert-butoxycarbonylamino-3-oxo-5-phenyl-pentanoic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591-87-7
Allyl acetate

: 1027300-21-5
2-benzyl-4-tert-butoxycarbonylamino-3-oxo-5-phenyl-pentanoic acid allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / carbonyl-1,1'-diimidazole; BuLi; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C

2: NaH / tetrahydrofuran / 2 h / Heating

With n-butyllithium; sodium hydride; diisopropylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran;
DOI:10.1021/jo010270f

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1027300-21-5
2-benzyl-4-tert-butoxycarbonylamino-3-oxo-5-phenyl-pentanoic acid allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / carbonyl-1,1'-diimidazole; BuLi; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C

2: NaH / tetrahydrofuran / 2 h / Heating

With n-butyllithium; sodium hydride; diisopropylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran;
DOI:10.1021/jo010270f