N-[(E)-2-(methylsulfonyl)-3-phenyl-2-propenyloxycarbonyloxy]succinimide

Base Information

Chemical Name:N-[(E)-2-(methylsulfonyl)-3-phenyl-2-propenyloxycarbonyloxy]succinimide
CAS No.:252668-50-1
Molecular Formula:C₁₅H₁₅NO₇S
Molecular Weight:353.353
Hs Code.:

Synonyms:N-[(E)-2-(methylsulfonyl)-3-phenyl-2-propenyloxycarbonyloxy]succinimide

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Chemical Property of N-[(E)-2-(methylsulfonyl)-3-phenyl-2-propenyloxycarbonyloxy]succinimide

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Technology Process of N-[(E)-2-(methylsulfonyl)-3-phenyl-2-propenyloxycarbonyloxy]succinimide

There total 3 articles about N-[(E)-2-(methylsulfonyl)-3-phenyl-2-propenyloxycarbonyloxy]succinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 82911-72-6
dicyclohexylamine salt of N-hydroxysuccinimide

: 252668-49-8
(E)-2-(methylsulfonyl)-3-phenyl-2-propenyl chloroformate

: 252668-50-1
N-[(E)-2-(methylsulfonyl)-3-phenyl-2-propenyloxycarbonyloxy]succinimide

Guidance literature:: In dichloromethane;
DOI:10.1021/jo990541a

Reference yield:

: (E)-3-bromo-2-(methylsulfonyl)-1-phenyl-1-propene

: 252668-50-1
N-[(E)-2-(methylsulfonyl)-3-phenyl-2-propenyloxycarbonyloxy]succinimide

Guidance literature:: Multi-step reaction with 3 steps

1: 80.2 percent / sodium formate; H₂O / methanol / 6 h / Heating

2: 86.4 percent / tetrahydrofuran / 20 °C

3: 75 percent / CH₂Cl₂

With water; sodium formate; In tetrahydrofuran; methanol; dichloromethane; 1: Substitution / 2: Substitution / 3: Substitution;
DOI:10.1021/jo990541a

Reference yield:

: 197244-90-9
(E)-2-(methylsulfonyl)-3-phenyl-2-propenyl alcohol

: 252668-50-1
N-[(E)-2-(methylsulfonyl)-3-phenyl-2-propenyloxycarbonyloxy]succinimide

Guidance literature:: Multi-step reaction with 2 steps

1: 86.4 percent / tetrahydrofuran / 20 °C

2: 75 percent / CH₂Cl₂

In tetrahydrofuran; dichloromethane; 1: Substitution / 2: Substitution;
DOI:10.1021/jo990541a