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carbonic acid allyl ester 2-(tert-butyl-dimethyl-silanyloxy)-cyclohex-1-enyl ester

Base Information Edit
  • Chemical Name:carbonic acid allyl ester 2-(tert-butyl-dimethyl-silanyloxy)-cyclohex-1-enyl ester
  • CAS No.:925462-07-3
  • Molecular Formula:C16H28O4Si
  • Molecular Weight:312.481
  • Hs Code.:
  • Mol file:925462-07-3.mol
carbonic acid allyl ester 2-(tert-butyl-dimethyl-silanyloxy)-cyclohex-1-enyl ester

Synonyms:carbonic acid allyl ester 2-(tert-butyl-dimethyl-silanyloxy)-cyclohex-1-enyl ester

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Chemical Property of carbonic acid allyl ester 2-(tert-butyl-dimethyl-silanyloxy)-cyclohex-1-enyl ester Edit
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Technology Process of carbonic acid allyl ester 2-(tert-butyl-dimethyl-silanyloxy)-cyclohex-1-enyl ester

There total 2 articles about carbonic acid allyl ester 2-(tert-butyl-dimethyl-silanyloxy)-cyclohex-1-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
carbonic acid allyl ester 2-oxo-cyclohexyl ester; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h;
tert-butyldimethylsilyl chloride; In tetrahydrofuran; at -78 - 20 ℃; for 1.5h;
DOI:10.1021/ja067342a
Guidance literature:
Multi-step reaction with 2 steps
1.1: 79 percent / pyridine / CH2Cl2 / 24 h / 0 - 20 °C
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C
2.2: 67 percent / tetrahydrofuran / 1.5 h / -78 - 20 °C
With pyridine; sodium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja067342a
Guidance literature:
With chiral ligand; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; In 1,4-dioxane; at 23 ℃; for 10h; Title compound not separated from byproducts;
DOI:10.1021/ja067342a
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