N-(2,5-dimethoxyphenylacetyl)-N'-(5-p-benzoyl-10,15,20-tri-p-tolylporphyrin)-1,2-diaminoethane

Base Information

Chemical Name:N-(2,5-dimethoxyphenylacetyl)-N'-(5-p-benzoyl-10,15,20-tri-p-tolylporphyrin)-1,2-diaminoethane
CAS No.:91289-48-4
Molecular Formula:C₆₀H₅₂N₆O₄
Molecular Weight:921.111
Hs Code.:

Synonyms:N-(2,5-dimethoxyphenylacetyl)-N'-(5-p-benzoyl-10,15,20-tri-p-tolylporphyrin)-1,2-diaminoethane

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Chemical Property of N-(2,5-dimethoxyphenylacetyl)-N'-(5-p-benzoyl-10,15,20-tri-p-tolylporphyrin)-1,2-diaminoethane

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Technology Process of N-(2,5-dimethoxyphenylacetyl)-N'-(5-p-benzoyl-10,15,20-tri-p-tolylporphyrin)-1,2-diaminoethane

There total 3 articles about N-(2,5-dimethoxyphenylacetyl)-N'-(5-p-benzoyl-10,15,20-tri-p-tolylporphyrin)-1,2-diaminoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1758-25-4
(2,5-dimethoxyphenyl)acetic acid

: 91289-48-4
N-(2,5-dimethoxyphenylacetyl)-N'-(5-p-benzoyl-10,15,20-tri-p-tolylporphyrin)-1,2-diaminoethane

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / K₂CO₃ / acetone / 5 h / Heating

2: 70 percent / 48 h / Ambient temperature

3: SOCl₂, pyridine / 1.)INO 1100+SOCl₂ reflux for 1 h. then evaporation under vacuum and the residue dissolve in CH₂Cl₂ 2.)INO 1150/CH₂Cl₂/pyridine+1.) on 0 deg C then stir at r.t. overnight

With pyridine; thionyl chloride; potassium carbonate; In acetone;

Reference yield:

: 6202-39-7
homogentisic acid methyl ester dimethyl ether

: 91289-48-4
N-(2,5-dimethoxyphenylacetyl)-N'-(5-p-benzoyl-10,15,20-tri-p-tolylporphyrin)-1,2-diaminoethane

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 48 h / Ambient temperature

2: SOCl₂, pyridine / 1.)INO 1100+SOCl₂ reflux for 1 h. then evaporation under vacuum and the residue dissolve in CH₂Cl₂ 2.)INO 1150/CH₂Cl₂/pyridine+1.) on 0 deg C then stir at r.t. overnight

With pyridine; thionyl chloride;

Reference yield:

: 61449-63-6
5-(4-Carboxyphenyl)-10,15,20-tris(4-methylphenyl) porphyrin

: 91289-41-7
N-(2,5-dimethoxyphenylacetyl)-1,2-diaminoethane

: 91289-48-4
N-(2,5-dimethoxyphenylacetyl)-N'-(5-p-benzoyl-10,15,20-tri-p-tolylporphyrin)-1,2-diaminoethane

Guidance literature:: With pyridine; thionyl chloride; Yield given. Multistep reaction; 1.)INO 1100+SOCl₂ reflux for 1 h. then evaporation under vacuum and the residue dissolve in CH₂Cl₂ 2.)INO 1150/CH₂Cl₂/pyridine+1.) on 0 deg C then stir at r.t. overnight;