S-(8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl)ethanethioate

Base Information

Chemical Name:S-(8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl)ethanethioate
CAS No.:896472-91-6
Molecular Formula:C₂₆H₄₁NO₄S
Molecular Weight:463.682
Hs Code.:

Synonyms:S-(8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl)ethanethioate

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Chemical Property of S-(8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl)ethanethioate

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Technology Process of S-(8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl)ethanethioate

There total 7 articles about S-(8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl)ethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 896472-89-2
8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl 4-methylbenzenesulfonate

: 10387-40-3
potassium thioacetate

: 896472-91-6
S-(8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl)ethanethioate

Guidance literature:: In ethanol; for 1h; Heating;
DOI:10.1016/j.bmc.2006.01.071

Reference yield:

: 896472-85-8
N-(2,2-dimethyl-5-(2-(4-(4-oxobutyl)phenyl)ethyl)-1,3-dioxan-5-yl)ethanamide

: 896472-91-6
S-(8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl)ethanethioate

Guidance literature:: Multi-step reaction with 5 steps

1: 52 percent / sodium hydride / dimethylformamide / 0.5 h / -25 °C

2: 99 percent / hydrogen / Pd/C / ethyl acetate / 2 h

3: 72 percent / lithium aluminum hydride / diethyl ether / 2 h / 20 °C

4: 81 percent / triethylamine / CH₂Cl₂ / 15 h / 20 °C

5: 94 percent / ethanol / 1 h / Heating

With lithium aluminium tetrahydride; hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 1: Wittig condensation;
DOI:10.1016/j.bmc.2006.01.071

Reference yield:

: ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)-2,4-octadienoate

: 896472-91-6
S-(8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octyl)ethanethioate

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / hydrogen / Pd/C / ethyl acetate / 2 h

2: 72 percent / lithium aluminum hydride / diethyl ether / 2 h / 20 °C

3: 81 percent / triethylamine / CH₂Cl₂ / 15 h / 20 °C

4: 94 percent / ethanol / 1 h / Heating

With lithium aluminium tetrahydride; hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmc.2006.01.071