N-(5-(2-(4-(8-hydroxyoctyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

Base Information

Chemical Name:N-(5-(2-(4-(8-hydroxyoctyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide
CAS No.:896472-87-0
Molecular Formula:C₂₄H₃₉NO₄
Molecular Weight:405.578
Hs Code.:

Synonyms:N-(5-(2-(4-(8-hydroxyoctyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(5-(2-(4-(8-hydroxyoctyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

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Technology Process of N-(5-(2-(4-(8-hydroxyoctyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

There total 5 articles about N-(5-(2-(4-(8-hydroxyoctyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 896472-86-9
ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)octanoate

: 896472-87-0
N-(5-(2-(4-(8-hydroxyoctyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2006.01.071

Reference yield:

: 896472-85-8
N-(2,2-dimethyl-5-(2-(4-(4-oxobutyl)phenyl)ethyl)-1,3-dioxan-5-yl)ethanamide

: 896472-87-0
N-(5-(2-(4-(8-hydroxyoctyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / sodium hydride / dimethylformamide / 0.5 h / -25 °C

2: 99 percent / hydrogen / Pd/C / ethyl acetate / 2 h

3: 72 percent / lithium aluminum hydride / diethyl ether / 2 h / 20 °C

With lithium aluminium tetrahydride; hydrogen; sodium hydride; palladium on activated charcoal; In diethyl ether; ethyl acetate; N,N-dimethyl-formamide; 1: Wittig condensation;
DOI:10.1016/j.bmc.2006.01.071

Reference yield:

: ethyl 8-(4-(2-(5-acetylamino-2,2-dimethyl-1,3-dioxan-5-yl)ethyl)phenyl)-2,4-octadienoate

: 896472-87-0
N-(5-(2-(4-(8-hydroxyoctyl)phenyl)ethyl)-2,2-dimethyl-1,3-dioxan-5-yl)ethanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / hydrogen / Pd/C / ethyl acetate / 2 h

2: 72 percent / lithium aluminum hydride / diethyl ether / 2 h / 20 °C

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; ethyl acetate;
DOI:10.1016/j.bmc.2006.01.071