6-[N-tert-Butyloxy-N-(2-nitrophenylsulfonyl)]aminohexanoic acid benzyl ester

Base Information

Chemical Name:6-[N-tert-Butyloxy-N-(2-nitrophenylsulfonyl)]aminohexanoic acid benzyl ester
CAS No.:359442-68-5
Molecular Formula:C₂₃H₃₀N₂O₇S
Molecular Weight:478.566
Hs Code.:

Synonyms:6-[N-tert-Butyloxy-N-(2-nitrophenylsulfonyl)]aminohexanoic acid benzyl ester

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Chemical Property of 6-[N-tert-Butyloxy-N-(2-nitrophenylsulfonyl)]aminohexanoic acid benzyl ester

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Technology Process of 6-[N-tert-Butyloxy-N-(2-nitrophenylsulfonyl)]aminohexanoic acid benzyl ester

There total 4 articles about 6-[N-tert-Butyloxy-N-(2-nitrophenylsulfonyl)]aminohexanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 78277-26-6
benzyl 6-bromohexanoate

: O-(1,1-Dimethylethyl)-N-(2-nitrophenylsulfonyl)hydroxylamine

: 359442-68-5
6-[N-tert-Butyloxy-N-(2-nitrophenylsulfonyl)]aminohexanoic acid benzyl ester

Guidance literature:: With caesium carbonate; In acetonitrile; for 6h; Heating;
DOI:10.1055/s-2001-14567

Reference yield:

: 4224-70-8
6-bromohexanoic acid

: 359442-68-5
6-[N-tert-Butyloxy-N-(2-nitrophenylsulfonyl)]aminohexanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / DIC; DMAP / tetrahydrofuran / 4.75 h / 0 - 20 °C

2: 100 percent / Cs₂CO₃ / acetonitrile / 6 h / Heating

With dmap; caesium carbonate; dacarbazine; In tetrahydrofuran; acetonitrile;
DOI:10.1055/s-2001-14567

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 359442-68-5
6-[N-tert-Butyloxy-N-(2-nitrophenylsulfonyl)]aminohexanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Et₃N / CHCl₃ / -5 - 20 °C

2: 100 percent / Cs₂CO₃ / acetonitrile / 6 h / Heating

With caesium carbonate; triethylamine; In chloroform; acetonitrile;
DOI:10.1055/s-2001-14567