Technology Process of N1-Benzyl-N2,1-diphenylethane-1,2-diamine
There total 4 articles about N1-Benzyl-N2,1-diphenylethane-1,2-diamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
aluminum (III) chloride; lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 3h;
DOI:10.1021/ol303302r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trimethylaluminum / toluene / 1 h / 0 - 20 °C
1.2: 20 h / 100 °C
2.1: copper diacetate; potassium phosphate; [bis(acetoxy)iodo]benzene / N,N-dimethyl-formamide / 6 h / 20 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride; aluminum (III) chloride / tetrahydrofuran / 3 h / 0 - 20 °C
With
aluminum (III) chloride; potassium phosphate; lithium aluminium tetrahydride; [bis(acetoxy)iodo]benzene; trimethylaluminum; copper diacetate;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol303302r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trimethylaluminum / toluene / 1 h / 0 - 20 °C
1.2: 20 h / 100 °C
2.1: copper diacetate; potassium phosphate; [bis(acetoxy)iodo]benzene / N,N-dimethyl-formamide / 6 h / 20 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride; aluminum (III) chloride / tetrahydrofuran / 3 h / 0 - 20 °C
With
aluminum (III) chloride; potassium phosphate; lithium aluminium tetrahydride; [bis(acetoxy)iodo]benzene; trimethylaluminum; copper diacetate;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol303302r
