(RSp)-allyl(N-methyl[(1RS,2SR)-(1-hydroxy-1-phenylprop-2-yl)]amino)phenyl-phosphine borane

Base Information

Chemical Name:(RSp)-allyl(N-methyl[(1RS,2SR)-(1-hydroxy-1-phenylprop-2-yl)]amino)phenyl-phosphine borane
CAS No.:294183-87-2
Molecular Formula:C₁₉H₂₇BNOP
Molecular Weight:327.214
Hs Code.:

Synonyms:(RSp)-allyl(N-methyl[(1RS,2SR)-(1-hydroxy-1-phenylprop-2-yl)]amino)phenyl-phosphine borane

Suppliers and Price of (RSp)-allyl(N-methyl[(1RS,2SR)-(1-hydroxy-1-phenylprop-2-yl)]amino)phenyl-phosphine borane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (RSp)-allyl(N-methyl[(1RS,2SR)-(1-hydroxy-1-phenylprop-2-yl)]amino)phenyl-phosphine borane

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Technology Process of (RSp)-allyl(N-methyl[(1RS,2SR)-(1-hydroxy-1-phenylprop-2-yl)]amino)phenyl-phosphine borane

There total 1 articles about (RSp)-allyl(N-methyl[(1RS,2SR)-(1-hydroxy-1-phenylprop-2-yl)]amino)phenyl-phosphine borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 264871-33-2,284662-93-7,294618-76-1,130666-29-4,190913-71-4
(2RS,4SR,5RS)-2,5-diphenyl-3,4-dimethyl-1,3,2-oxazaphospholidine-2-borane

: 3052-45-7
allyllithium

: 294183-87-2
(RSp)-allyl(N-methyl[(1RS,2SR)-(1-hydroxy-1-phenylprop-2-yl)]amino)phenyl-phosphine borane

Guidance literature:: In tetrahydrofuran; -78°C;
DOI:10.1002/1521-3773(20000717)39:14<2491::AID-ANIE2491>3.0.CO;2-H

Reference yield: 79.0%

: 67-56-1
methanol

: 294183-87-2
(RSp)-allyl(N-methyl[(1RS,2SR)-(1-hydroxy-1-phenylprop-2-yl)]amino)phenyl-phosphine borane

: 920017-02-3
allyl(methoxy)phenylphosphine borane

Guidance literature:: With sulfuric acid; In methanol; byproducts: ephedrine hydrochloride; (Ar); concd. H2SO4 was added to soln. of P-B compd. in MeOH; stirred at room temp. overnight; MeOH removed (vac.); stirred in Et2O for several min; filtered; solvent removed (vac.); chromd. (silica gel, hexane/EtOAc, 4/1);
DOI:10.1016/j.jorganchem.2006.08.084