Pd(dpmp)2Cl₂

Base Information

Chemical Name:Pd(dpmp)2Cl₂
CAS No.:84751-00-8
Molecular Formula:C₃₂H₂₉Cl₂P₃Pd
Molecular Weight:683.83
Hs Code.:

Synonyms:Pd(dpmp)2Cl₂

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Chemical Property of Pd(dpmp)2Cl₂

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Technology Process of Pd(dpmp)2Cl₂

There total 1 articles about Pd(dpmp)2Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 2071-24-1
bis(diphenylphosphinomethyl)phenylphosphine

: 84751-00-8
Pd(dpmp)2Cl₂

Guidance literature:: In dichloromethane; equimolar amounts of the organic ligand and the Pd-complex; diethyl ether was added;
DOI:10.1021/ja00344a057

Reference yield: 92.0%

: tetracarbonyldi-μ-chlorodirhodium(I)

: 84751-00-8
[Pd(((C₆H₅)2PCH₂)2PC₆H₅)Cl₂]

: 93921-90-5
Rh(CO)Cl[(((C₆H₅)2PCH₂)2PC₆H₅)PdCl₂]2

Guidance literature:: In dichloromethane; a soln. of reagents was stirred for 0.5 h; ppt. was filtered, washed with ether; elem.anal.;

Reference yield: 82.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 84751-00-8
Pd(dpmp)2Cl₂

: chloro-(η4-cycloocta-1,5-diene)-{cis-(bis(diphenylphosphinomethyl)phenylphosphine)(dichloropalladium(II))}-rhodium(I)

Guidance literature:: In dichloromethane; A soln. of Rh2Cl2(C8H12)2 complex is added to a soln. of phosphine complex (1:2 molar ratio), the reaction mixture is stirred under N2 for 1 h.; addn. of diethyl ether, filtn., washing with diethyl ether, drying in vacuo, elem. anal.;