N,N-Bis-(2-ethylthio)-ethylaniline

Base Information

Chemical Name:N,N-Bis-(2-ethylthio)-ethylaniline
CAS No.:148932-04-1
Molecular Formula:C₁₄H₂₃NS₂
Molecular Weight:269.475
Hs Code.:
European Community (EC) Number:652-100-4
Nikkaji Number:J1.065.586B

Synonyms:N,N-BIS-(2-ETHYLTHIO)-ETHYLANILINE;SCHEMBL9326900;6-Phenyl-3,9-dithia-6-azaundecane;AKOS024323733

Suppliers and Price of N,N-Bis-(2-ethylthio)-ethylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-Bis-(2-ethylthio)-ethylaniline

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:9
Exact Mass:269.12719208
Heavy Atom Count:17
Complexity:160

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCSCCN(CCSCC)C1=CC=CC=C1

Technology Process of N,N-Bis-(2-ethylthio)-ethylaniline

There total 4 articles about N,N-Bis-(2-ethylthio)-ethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: bis(2-tosylethyl)phenylamine

: 75-08-1
ethanethiol

: 148932-04-1
6-phenyll-3,9-dithia-6-azaundecane

Guidance literature:: ethanethiol; With sodium; In ethanol; for 0.25h; Inert atmosphere; Schlenk technique;

bis(2-tosylethyl)phenylamine; In tetrahydrofuran; ethanol; at 0 ℃; for 2h; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1016/j.ica.2018.04.033

Reference yield:

: 120-07-0
2,2'-(phenylimino)bis[ethanol]

: 148932-04-1
6-phenyll-3,9-dithia-6-azaundecane

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / NaOH / H₂O; tetrahydrofuran

2: 1.) NaOEt / 1.) ethanol, RT, 1 h, 2.) ethanol, 12 h

With sodium hydroxide; sodium ethanolate; In tetrahydrofuran; water;
DOI:10.1246/bcsj.68.3071

Reference yield:

: 3590-12-3
N,N-bis(2-p-tolylsulfonyloxyethyl)aniline

: 75-08-1
ethanethiol

: 148932-04-1
6-phenyll-3,9-dithia-6-azaundecane

Guidance literature:: With sodium ethanolate; Yield given. Multistep reaction; 1.) ethanol, RT, 1 h, 2.) ethanol, 12 h;
DOI:10.1246/bcsj.68.3071