1-(2-benzylbenzyl)-3-(4-methoxybenzyl)-5,5-dimethylimidazolidine-2,4-dione

Base Information

Chemical Name:1-(2-benzylbenzyl)-3-(4-methoxybenzyl)-5,5-dimethylimidazolidine-2,4-dione
CAS No.:1179804-61-5
Molecular Formula:C₂₇H₂₈N₂O₃
Molecular Weight:428.531
Hs Code.:

Synonyms:1-(2-benzylbenzyl)-3-(4-methoxybenzyl)-5,5-dimethylimidazolidine-2,4-dione

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Chemical Property of 1-(2-benzylbenzyl)-3-(4-methoxybenzyl)-5,5-dimethylimidazolidine-2,4-dione

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Technology Process of 1-(2-benzylbenzyl)-3-(4-methoxybenzyl)-5,5-dimethylimidazolidine-2,4-dione

There total 3 articles about 1-(2-benzylbenzyl)-3-(4-methoxybenzyl)-5,5-dimethylimidazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 55276-42-1
2-benzylbenzyl bromide

: 220615-80-5
3-(4-methoxybenzyl)-5,5-dimethylimidazolidine-2,4-dione

: 1179804-61-5
1-(2-benzylbenzyl)-3-(4-methoxybenzyl)-5,5-dimethylimidazolidine-2,4-dione

Guidance literature:: With caesium carbonate; In acetonitrile; at 75 ℃; for 6h;

Reference yield:

: 1586-00-1
2-(benzyl)benzyl alcohol

: 1179804-61-5
1-(2-benzylbenzyl)-3-(4-methoxybenzyl)-5,5-dimethylimidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole; triphenylphosphine; bromine / dichloromethane / 5 - 20 °C

2: caesium carbonate / acetonitrile / 6 h / 75 °C

With 1H-imidazole; bromine; caesium carbonate; triphenylphosphine; In dichloromethane; acetonitrile;

Reference yield:

: 77-71-4
5,5-dimethyl-imidazolidine-2,4-dione

: 824-94-2
p-methoxybenzyl chloride

: 1179804-61-5
1-(2-benzylbenzyl)-3-(4-methoxybenzyl)-5,5-dimethylimidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 8 h / 20 °C / Inert atmosphere

2: caesium carbonate / acetonitrile / 6 h / 75 °C

With potassium carbonate; caesium carbonate; In acetonitrile;