4-(5-chloro-2-isopropylamino-pyridin-4-yl)-1-(2,4,6-trimethyl-benzenesulfonyl)-1H-pyrrole-2-carboxylic acid methyl ester N-oxide

Base Information

Chemical Name:4-(5-chloro-2-isopropylamino-pyridin-4-yl)-1-(2,4,6-trimethyl-benzenesulfonyl)-1H-pyrrole-2-carboxylic acid methyl ester N-oxide
CAS No.:869886-92-0
Molecular Formula:C₂₃H₂₆ClN₃O₅S
Molecular Weight:491.996
Hs Code.:

Synonyms:4-(5-chloro-2-isopropylamino-pyridin-4-yl)-1-(2,4,6-trimethyl-benzenesulfonyl)-1H-pyrrole-2-carboxylic acid methyl ester N-oxide

Suppliers and Price of 4-(5-chloro-2-isopropylamino-pyridin-4-yl)-1-(2,4,6-trimethyl-benzenesulfonyl)-1H-pyrrole-2-carboxylic acid methyl ester N-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(5-chloro-2-isopropylamino-pyridin-4-yl)-1-(2,4,6-trimethyl-benzenesulfonyl)-1H-pyrrole-2-carboxylic acid methyl ester N-oxide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(5-chloro-2-isopropylamino-pyridin-4-yl)-1-(2,4,6-trimethyl-benzenesulfonyl)-1H-pyrrole-2-carboxylic acid methyl ester N-oxide

There total 4 articles about 4-(5-chloro-2-isopropylamino-pyridin-4-yl)-1-(2,4,6-trimethyl-benzenesulfonyl)-1H-pyrrole-2-carboxylic acid methyl ester N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53976-62-8
2,5-dichloro-1-oxido-pyridin-1-ium

: 869886-92-0
4-(5-chloro-2-isopropylamino-pyridin-4-yl)-1-(2,4,6-trimethyl-benzenesulfonyl)-1H-pyrrole-2-carboxylic acid methyl ester N-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; nitric acid / 1.5 h / 100 °C

2: Acetyl bromide / 0.17 h / 80 °C

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; benzene / 16 h / 80 °C / Heating / reflux

With Acetyl bromide; sulfuric acid; nitric acid; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; benzene;

Reference yield:

: 405230-81-1
2,5-dichloro-4-nitropyridine-1-oxide

: 869886-92-0
4-(5-chloro-2-isopropylamino-pyridin-4-yl)-1-(2,4,6-trimethyl-benzenesulfonyl)-1H-pyrrole-2-carboxylic acid methyl ester N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: Acetyl bromide / 0.17 h / 80 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; benzene / 16 h / 80 °C / Heating / reflux

With Acetyl bromide; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; benzene;

Reference yield:

: 16110-09-1
2,5 dichloropyridine

: 869886-92-0
4-(5-chloro-2-isopropylamino-pyridin-4-yl)-1-(2,4,6-trimethyl-benzenesulfonyl)-1H-pyrrole-2-carboxylic acid methyl ester N-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: dihydrogen peroxide; acetic anhydride / water / 54 h / 20 - 60 °C

2: sulfuric acid; nitric acid / 1.5 h / 100 °C

3: Acetyl bromide / 0.17 h / 80 °C

4: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; benzene / 16 h / 80 °C / Heating / reflux

With Acetyl bromide; sulfuric acid; dihydrogen peroxide; nitric acid; acetic anhydride; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; benzene;