Technology Process of 4-benzyloxy-2-nitrobenzenesulfonyl chloride
There total 3 articles about 4-benzyloxy-2-nitrobenzenesulfonyl chloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-benzyloxy-2-nitroaniline;
With
hydrogenchloride; trifluoroacetic acid; sodium nitrite;
at 0 ℃;
for 0.0833333h;
With
sulphurous acid; acetic acid; copper dichloride;
copper(l) chloride;
at 20 ℃;
for 0.583333h;
DOI:10.1021/jm020475w
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butoxide / dimethylformamide / 0.5 h / 0 °C
1.2: 81 percent / dimethylformamide / 0.5 h / 0 °C
2.1: TFA; aq. HCl; NaNO2 / 0.08 h / 0 °C
2.2: 75 percent / aq. AcOH; H2SO3; CuCl2 / CuCl / 0.58 h / 20 °C
With
hydrogenchloride; potassium tert-butylate; trifluoroacetic acid; sodium nitrite;
In
N,N-dimethyl-formamide;
DOI:10.1021/jm020475w
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butoxide / dimethylformamide / 0.5 h / 0 °C
1.2: 81 percent / dimethylformamide / 0.5 h / 0 °C
2.1: TFA; aq. HCl; NaNO2 / 0.08 h / 0 °C
2.2: 75 percent / aq. AcOH; H2SO3; CuCl2 / CuCl / 0.58 h / 20 °C
With
hydrogenchloride; potassium tert-butylate; trifluoroacetic acid; sodium nitrite;
In
N,N-dimethyl-formamide;
DOI:10.1021/jm020475w
