4-BENZYLOXY-2-NITROANILINE

Base Information

• Chemical Name: 4-BENZYLOXY-2-NITROANILINE
• CAS No.: 26697-35-8
• Molecular Formula: C13H12N2O3
• Molecular Weight: 244.25
• Hs Code.: 2922199090
• Mol file: 26697-35-8.mol

Synonyms:2-nitro-4-phenylmethoxyaniline;

Chemical Property of 4-BENZYLOXY-2-NITROANILINE

Chemical Property:

• Vapor Pressure: 4.59E-08mmHg at 25°C
• Melting Point: 141-143oC
• Boiling Point: 443.6°C at 760 mmHg
• PKA: 0.90±0.10(Predicted)
• Flash Point: 222.1°C
• PSA: 81.07000
• Density: 1.297g/cm³
• LogP: 3.86040
• Storage Temp.: Refrigerator
• Solubility.: Chloroform, Dichloromethane, Ethyl Acetate, Methanol

Purity/Quality:

97% ^*data from raw suppliers

4-Benzyloxy-2-nitroaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Total 1 MSDS from other Authors

Useful:

Technology Process of 4-BENZYLOXY-2-NITROANILINE

There total 9 articles about 4-BENZYLOXY-2-NITROANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.6%

4-hydroxy-2-nitroaniline (610-81-1) + benzyl bromide (100-39-0) → 4-benzyloxy-2-nitroaniline (26697-35-8)

Guidance literature:

With potassium carbonate; In acetone; at 0 - 20 ℃; for 12h;

Reference yield: 86.0%

N-(4-(benzyloxy)-2-nitrophenyl)acetamide (26697-34-7) → 4-benzyloxy-2-nitroaniline (26697-35-8)

Guidance literature:

With hydrogenchloride; water; In ethanol; for 6h; Reflux; Inert atmosphere;

DOI:10.1039/b924619c

Reference yield: 58.0%

4-hydroxy-2-nitroaniline (610-81-1) → 4-benzyloxy-2-nitroaniline (26697-35-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; chemoselective reaction;

DOI:10.1021/jm301124s

upstream raw materials:

N-(4-(benzyloxy)-2-nitrophenyl)acetamide

4-hydroxy-2-nitroaniline

benzyl chloride

benzyl bromide

Downstream raw materials:

4-(benzyloxy)-1,2-phenylenediamine

4-benzyloxy-2-nitrobenzenesulfonyl chloride

methyl 2-{[4-(benzyloxy)-2-nitrophenyl]amino}-4-chlorobenzoate

methyl 2-(2-amino-4-(benzyloxy)phenylamino)-4-chlorobenzoate

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