Technology Process of C30H29N7O6S
There total 5 articles about C30H29N7O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
bis(trichloromethyl) carbonate; C22H27NO4;
With
triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 0.25h;
C7H4N6OS;
With
dmap;
In
toluene;
at 70 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 - 80 °C / Inert atmosphere
1.2: pH 1
2.1: potassium carbonate / sodium iodide / N,N-dimethyl-formamide; acetone / 6 h / 20 - 70 °C / Inert atmosphere
3.1: caesium carbonate; copper(l) iodide; 2-(2-methyl-1-oxopropane)cyclohexanone / N,N-dimethyl-formamide / 1 h / 100 °C / Inert atmosphere; Microwave irradiation; Sealed tube
4.1: triethylamine / dichloromethane / 0.25 h / 0 - 20 °C
4.2: 16 h / 70 °C
With
copper(l) iodide; 2-(2-methyl-1-oxopropane)cyclohexanone; water; potassium carbonate; caesium carbonate; triethylamine; lithium hydroxide;
sodium iodide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / sodium iodide / N,N-dimethyl-formamide; acetone / 6 h / 20 - 70 °C / Inert atmosphere
2.1: caesium carbonate; copper(l) iodide; 2-(2-methyl-1-oxopropane)cyclohexanone / N,N-dimethyl-formamide / 1 h / 100 °C / Inert atmosphere; Microwave irradiation; Sealed tube
3.1: triethylamine / dichloromethane / 0.25 h / 0 - 20 °C
3.2: 16 h / 70 °C
With
copper(l) iodide; 2-(2-methyl-1-oxopropane)cyclohexanone; potassium carbonate; caesium carbonate; triethylamine;
sodium iodide;
In
dichloromethane; N,N-dimethyl-formamide; acetone;