Furil monotosylhydrazone

Base Information

• Chemical Name: Furil monotosylhydrazone
• CAS No.: 165754-86-9
• Molecular Formula: C₁₇H₁₄N₂O₅S
• Molecular Weight: 358.375
• Mol file: 165754-86-9.mol

Synonyms:Furil monotosylhydrazone

Chemical Property of Furil monotosylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Furil monotosylhydrazone

There total 1 articles about Furil monotosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

furil (492-94-4) + toluene-4-sulfonic acid hydrazide (1576-35-8) → Furil monotosylhydrazone (165754-86-9) + Furil bistosylhydrazone

Guidance literature:

In benzene; at 45 ℃; for 96h; Yields of byproduct given;

DOI:10.1021/jo00118a012

Reference yield: 76.0%

Furil monotosylhydrazone (165754-86-9) + benzylamine (100-46-9) → 1-Benzyl-5-(2-furoylmethylene)pyrrolidin-2-one

Guidance literature:

With sodium carbonate; In dichloromethane; for 48h; Ambient temperature;

DOI:10.1021/jo00118a012

Reference yield: 60.0%

phenylhydrazine (100-63-0) + Furil monotosylhydrazone (165754-86-9) → 1-(2-Furoyl)-6-anilino-6-azafulvene

Guidance literature:

With sodium carbonate; In benzene; for 48h; Ambient temperature;

DOI:10.1021/jo00118a012

upstream raw materials:

furil

toluene-4-sulfonic acid hydrazide