N-tert-butylhexanamide

Base Information

• Chemical Name: N-tert-butylhexanamide
• CAS No.: 1190-31-4
• Molecular Formula: C₁₀H₂₁NO
• Molecular Weight: 171.283
• Mol file: 1190-31-4.mol

Synonyms:Hexanamide,N-tert-butyl- (7CI,8CI); NSC 74544

Chemical Property of N-tert-butylhexanamide

Chemical Property:

• Vapor Pressure: 0.0282mmHg at 25°C
• Boiling Point: 245.8°C at 760 mmHg
• Flash Point: 140.8°C
• Density: 0.858g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-tert-butylhexanamide

There total 3 articles about N-tert-butylhexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C10H21NO → N-tert-butylcaproamide (1190-31-4)

Guidance literature:

With trifluoroacetic acid; 9?mesityl-10-methylacridinium perchlorate; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere; Irradiation;

DOI:10.1039/d1cc03855a

Reference yield:

hexanal (66-25-1) → N-tert-butylcaproamide (1190-31-4)

Guidance literature:

Multi-step reaction with 2 steps

1: dihydrogen peroxide / Inert atmosphere

2: 9?mesityl-10-methylacridinium perchlorate; trifluoroacetic acid / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere; Irradiation

With dihydrogen peroxide; trifluoroacetic acid; 9?mesityl-10-methylacridinium perchlorate; In N,N-dimethyl-formamide;

DOI:10.1039/d1cc03855a

Reference yield:

Hexanoyl chloride (142-61-0) + tert-butylamine (75-64-9) → N-tert-butylcaproamide (1190-31-4)

Guidance literature:

DOI:10.1021/jo01022a022

upstream raw materials:

Hexanoyl chloride

tert-butylamine

hexanal