C₆H₅CH₂SCo(CO)4

Base Information

Chemical Name:C₆H₅CH₂SCo(CO)4
CAS No.:130585-90-9
Molecular Formula:C₁₁H₇CoO₄S
Molecular Weight:294.233
Hs Code.:

C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>SCo(CO)4

Synonyms:C₆H₅CH₂SCo(CO)4

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Chemical Property of C₆H₅CH₂SCo(CO)4

Chemical Property:

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Technology Process of C₆H₅CH₂SCo(CO)4

There total 2 articles about C₆H₅CH₂SCo(CO)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15976-97-3
tetracarbonyl iodo cobalt

: 3492-64-6
sodium benzylmercaptide

: 130585-90-9
C₆H₅CH₂SCo(CO)4

Guidance literature:: With 5-crown-15; In tetrahydrofuran; addn. of 5-crown-15 soln. and PhCH2SNa to Co complex soln. at -80°C carefully excluding air and moisture; color change within a few min; complete conversion within 20-80 min; detn. by IR;

Reference yield:

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 882-33-7
diphenyldisulfane

: 130585-90-9
C₆H₅CH₂SCo(CO)4

Guidance literature:: In tetrahydrofuran; addn. of a cold soln. of diphenyldisulfide to a soln. of Co2(CO)8 in THF, cooled to -80 ° C; while stirring, the mixt. was kept at -80 °C for 30 min, then allowed to warm to -40 degree.C; After 2 h at -40 °C the react. is complete;;

Reference yield: 79.0%

: 130585-90-9
C₆H₅CH₂SCo(CO)4

: 130585-94-3
C₆H₅CH₂SCo(CO)3P(C₆H₅)3

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; addn. of Ph3P to Co complex soln. at -40°C carefully excluding air and moisture; stirring at -40°C, 60-80 min; chilling to -80°C; detn. by IR; layering pentane over soln.; standing overnight, -80°C; pptn. decantation; filtration; washing (n-pentane); elem. anal.;