(η4-exo-1-hydroxy-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron

Base Information

Chemical Name:(η4-exo-1-hydroxy-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron
CAS No.:112296-20-5
Molecular Formula:C₂₀H₁₆FeO₄Si
Molecular Weight:404.277
Hs Code.:

Synonyms:(η4-exo-1-hydroxy-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron

Suppliers and Price of (η4-exo-1-hydroxy-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron

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Chemical Property of (η4-exo-1-hydroxy-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron

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Technology Process of (η4-exo-1-hydroxy-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron

There total 3 articles about (η4-exo-1-hydroxy-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 112296-19-2
(η4-exo-1-chloro-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron

: 112296-20-5
(η4-exo-1-hydroxy-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron

Guidance literature:: With H₂O; In acetone; water added to a mixt. of complex in acetone, mixt. stireed (0.5h, room temp.); exclusion of air and moisture; solvent removed (vac.), recrystn. (hexane, -20°C);

Reference yield: 90.0%

: 112296-18-1
(η4-exo-1-hydro-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron

: 112296-20-5
(η4-exo-1-hydroxy-endo-1-methyl-2,5-diphenylsilacyclopentadiene)tricarbonyliron

Guidance literature:: With H₂O; In acetone; addn. of water to soln. of Fe-compd., stirred (3h, 42°C), solvents pumped off, residue extd. with hot hexane, exclusion of air and moisture; filtration, concd., cooled to -20°C; elem. anal.;

Reference yield: 72.0%

: 112218-89-0,112296-19-2
(η4-1-methyl-1-chloro-2,5-diphenylsilacyclopentadiene)tricarbonyliron

: 112218-90-3,112296-20-5
(η4-1-methyl-1-hydroxy-2,5-diphenylsilacyclopentadiene)tricarbonyliron

Guidance literature:: With H₂O; In acetone; exclusion of air and moisture; H2O added to complex, stirred (3h, room temp.); isomer ratio endo:exo =65:35; solvent removed (vac.), recrystn. (hexane, -20°C); H-NMR;