1,10-bis(2'-benzoyl chloride)-1,4,7,10-tetraoxadecane

Base Information

Chemical Name:1,10-bis(2'-benzoyl chloride)-1,4,7,10-tetraoxadecane
CAS No.:201596-37-4
Molecular Formula:C₂₀H₂₀Cl₂O₆
Molecular Weight:427.281
Hs Code.:

Synonyms:1,10-bis(2'-benzoyl chloride)-1,4,7,10-tetraoxadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,10-bis(2'-benzoyl chloride)-1,4,7,10-tetraoxadecane

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Technology Process of 1,10-bis(2'-benzoyl chloride)-1,4,7,10-tetraoxadecane

There total 7 articles about 1,10-bis(2'-benzoyl chloride)-1,4,7,10-tetraoxadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 74145-30-5
1,10-bis(2'-carboxylphenyl)-1,4,7,10-tetraoxadecane

: 201596-37-4
1,10-bis(2'-benzoyl chloride)-1,4,7,10-tetraoxadecane

Guidance literature:: With thionyl chloride; at 50 - 60 ℃; for 4h;
DOI:10.1021/jo971453y

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 201596-37-4
1,10-bis(2'-benzoyl chloride)-1,4,7,10-tetraoxadecane

Guidance literature:: Multi-step reaction with 3 steps

1: t-BuOK / tetrahydrofuran

2: aq. NaOH

3: SOCl₂ / 3 h / Heating

With sodium hydroxide; thionyl chloride; potassium tert-butylate; In tetrahydrofuran;
DOI:10.1021/jp981567t

Reference yield:

: 31255-10-4
1,2-bis-(2-bromo-ethoxy)-ethane

: 201596-37-4
1,10-bis(2'-benzoyl chloride)-1,4,7,10-tetraoxadecane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / Heating

2: Alkaline hydrolysis

3: thionyl chloride / Heating

With thionyl chloride; potassium carbonate; In acetone;