15-[(4-Benzyloxycarbonylamino-butyl)-(3-benzyloxycarbonylamino-propyl)-carbamoyl]-pentadecanoic acid methyl ester

Base Information

Chemical Name:15-[(4-Benzyloxycarbonylamino-butyl)-(3-benzyloxycarbonylamino-propyl)-carbamoyl]-pentadecanoic acid methyl ester
CAS No.:177334-74-6
Molecular Formula:C₄₀H₆₁N₃O₇
Molecular Weight:695.94
Hs Code.:

Synonyms:15-[(4-Benzyloxycarbonylamino-butyl)-(3-benzyloxycarbonylamino-propyl)-carbamoyl]-pentadecanoic acid methyl ester

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Chemical Property of 15-[(4-Benzyloxycarbonylamino-butyl)-(3-benzyloxycarbonylamino-propyl)-carbamoyl]-pentadecanoic acid methyl ester

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Technology Process of 15-[(4-Benzyloxycarbonylamino-butyl)-(3-benzyloxycarbonylamino-propyl)-carbamoyl]-pentadecanoic acid methyl ester

There total 4 articles about 15-[(4-Benzyloxycarbonylamino-butyl)-(3-benzyloxycarbonylamino-propyl)-carbamoyl]-pentadecanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 18451-85-9
15-(methoxycarbonyl)pentadecanoic acid

: 89965-56-0
<3-<<4-(carboxyamino)butyl>amino>propyl>carbamic acid, dibenzyl ester

: 177334-74-6
15-[(4-Benzyloxycarbonylamino-butyl)-(3-benzyloxycarbonylamino-propyl)-carbamoyl]-pentadecanoic acid methyl ester

Guidance literature:: With 2-chloro-1-methyl-pyridinium iodide; triethylamine; In dichloromethane; reflux, 1.5 h; 23 deg C, overnight;
DOI:10.1002/hlca.19960790221

Reference yield:

: 124-20-9
N-(3-aminopropyl)-1,4-diaminobutane

: 177334-74-6
15-[(4-Benzyloxycarbonylamino-butyl)-(3-benzyloxycarbonylamino-propyl)-carbamoyl]-pentadecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / CHCl₃ / 16 h / 23 °C

2: 96 percent / 1-methyl-2-chloropyridiniumiodide, Et₃N / CH₂Cl₂ / reflux, 1.5 h; 23 deg C, overnight

With 2-chloro-1-methyl-pyridinium iodide; triethylamine; In dichloromethane; chloroform;
DOI:10.1002/hlca.19960790221

Reference yield:

: 506-13-8
16-hydroxyhexadecanoic acid

: 177334-74-6
15-[(4-Benzyloxycarbonylamino-butyl)-(3-benzyloxycarbonylamino-propyl)-carbamoyl]-pentadecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / methanol

2: 97 percent / chromic acid / acetone / 3 h

3: 96 percent / 1-methyl-2-chloropyridiniumiodide, Et₃N / CH₂Cl₂ / reflux, 1.5 h; 23 deg C, overnight

With 2-chloro-1-methyl-pyridinium iodide; chromic acid; triethylamine; In methanol; dichloromethane; acetone;
DOI:10.1002/hlca.19960790221