C₂₂H₁₈FN₂O₂P

Base Information

Chemical Name:C₂₂H₁₈FN₂O₂P
CAS No.:692754-62-4
Molecular Formula:C₂₂H₁₈FN₂O₂P
Molecular Weight:392.369
Hs Code.:

C<sub>22</sub>H<sub>18</sub>FN<sub>2</sub>O<sub>2</sub>P

Synonyms:C₂₂H₁₈FN₂O₂P

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Chemical Property of C₂₂H₁₈FN₂O₂P

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Technology Process of C₂₂H₁₈FN₂O₂P

There total 2 articles about C₂₂H₁₈FN₂O₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 7677-24-9
trimethylsilyl cyanide

: C₂₁H₁₇FNO₂P

: 692754-62-4
C₂₂H₁₈FN₂O₂P

Guidance literature:: With gadolinium(III) isopropoxide; 2.6-dimethylphenol; 1,5-anhydro-2,6-dideoxy-3-O-(4,5-difluoro-2-hydroxyphenyl)-6-(diphenylphosphinyl)-D-arabino-hexitol; In various solvent(s); at -40 ℃; for 83h;
DOI:10.1016/j.tetlet.2004.02.082

Reference yield:

: 74-90-8
hydrogen cyanide

: C₂₁H₁₇FNO₂P

: 692754-62-4
C₂₂H₁₈FN₂O₂P

: C₂₂H₁₈FN₂O₂P

Guidance literature:: With trimethylsilyl cyanide; Gd(iPr)3; 1,5-anhydro-2,6-dideoxy-3-O-(4,5-difluoro-2-hydroxyphenyl)-6-(diphenylphosphinyl)-D-arabino-hexitol; In various solvent(s); at -40 ℃; for 1.3h; Title compound not separated from byproducts.;
DOI:10.1016/j.tetlet.2004.02.077

Reference yield:

: 692754-62-4
C₂₂H₁₈FN₂O₂P

: 67146-05-8,69684-83-9,69881-27-2,113387-54-5,68367-52-2
sorbinil

Guidance literature:: Multi-step reaction with 2 steps

1.1: 86 percent / conc. HCl / 16 h / Heating

2.1: H₂O / 14 h / 80 °C

2.2: conc. HCl / 8 h / Heating

With hydrogenchloride; In water;
DOI:10.1016/j.tetlet.2004.02.082