4-(2,5-Dimethoxy-benzyl)-5,6-dihydro-4H-benzo[f]pyrrolo[1,2-a][1,4]diazepine

Base Information

Chemical Name:4-(2,5-Dimethoxy-benzyl)-5,6-dihydro-4H-benzo[f]pyrrolo[1,2-a][1,4]diazepine
CAS No.:171413-59-5
Molecular Formula:C₂₁H₂₂N₂O₂
Molecular Weight:334.418
Hs Code.:

Synonyms:4-(2,5-Dimethoxy-benzyl)-5,6-dihydro-4H-benzo[f]pyrrolo[1,2-a][1,4]diazepine

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Chemical Property of 4-(2,5-Dimethoxy-benzyl)-5,6-dihydro-4H-benzo[f]pyrrolo[1,2-a][1,4]diazepine

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Technology Process of 4-(2,5-Dimethoxy-benzyl)-5,6-dihydro-4H-benzo[f]pyrrolo[1,2-a][1,4]diazepine

There total 4 articles about 4-(2,5-Dimethoxy-benzyl)-5,6-dihydro-4H-benzo[f]pyrrolo[1,2-a][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1027045-32-4
4-(2,5-Dimethoxy-benzyl)-6H-benzo[f]pyrrolo[1,2-a][1,4]diazepine

: 171413-59-5
4-(2,5-Dimethoxy-benzyl)-5,6-dihydro-4H-benzo[f]pyrrolo[1,2-a][1,4]diazepine

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 48h; Yield given; Ambient temperature;
DOI:10.1016/0223-5234(96)88274-2

Reference yield:

: 39243-88-4
2-(1-pyrrolyl)benzylamine

: 171413-59-5
4-(2,5-Dimethoxy-benzyl)-5,6-dihydro-4H-benzo[f]pyrrolo[1,2-a][1,4]diazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / triethylamine, N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide hydrochloride / 2 h / Ambient temperature

2: phosphoryl chloride / 2 h / 40 °C

3: sodium borohydride / aq. ethanol / 48 h / Ambient temperature

With sodium tetrahydroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trichlorophosphate; In ethanol;
DOI:10.1016/0223-5234(96)88274-2

Reference yield:

: 1758-25-4
(2,5-dimethoxyphenyl)acetic acid

: 171413-59-5
4-(2,5-Dimethoxy-benzyl)-5,6-dihydro-4H-benzo[f]pyrrolo[1,2-a][1,4]diazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / triethylamine, N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide hydrochloride / 2 h / Ambient temperature

2: phosphoryl chloride / 2 h / 40 °C

3: sodium borohydride / aq. ethanol / 48 h / Ambient temperature

With sodium tetrahydroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trichlorophosphate; In ethanol;
DOI:10.1016/0223-5234(96)88274-2