6-(2,4-dichlorophenyl)-3-[4-(methylsulfonyl)benzyl]-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

Base Information

Chemical Name:6-(2,4-dichlorophenyl)-3-[4-(methylsulfonyl)benzyl]-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine
CAS No.:1394240-77-7
Molecular Formula:C₁₈H₁₄Cl₂N₄O₂S₂
Molecular Weight:453.373
Hs Code.:

Synonyms:6-(2,4-dichlorophenyl)-3-[4-(methylsulfonyl)benzyl]-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

Suppliers and Price of 6-(2,4-dichlorophenyl)-3-[4-(methylsulfonyl)benzyl]-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-(2,4-dichlorophenyl)-3-[4-(methylsulfonyl)benzyl]-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-(2,4-dichlorophenyl)-3-[4-(methylsulfonyl)benzyl]-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

There total 4 articles about 6-(2,4-dichlorophenyl)-3-[4-(methylsulfonyl)benzyl]-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1394240-72-2
4-amino-5-[4-(methylsulfonyl)benzyl]-2,4-dihydro-3H-[1,2,4]-triazole-3-thione

: 2631-72-3
2,4-dichlorophenacyl bromide

: 1394240-77-7
6-(2,4-dichlorophenyl)-3-[4-(methylsulfonyl)benzyl]-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

Guidance literature:: In ethanol; at 80 ℃; for 5h;
DOI:10.1016/j.ejmech.2012.04.024

Reference yield:

: 90536-66-6
4-(methylsulfonyl)phenylacetic acid

: 1394240-77-7
6-(2,4-dichlorophenyl)-3-[4-(methylsulfonyl)benzyl]-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 80 °C

2.1: hydrazine hydrate / ethanol / 10 h / 80 °C

3.1: potassium hydroxide / ethanol / 10 h / 20 °C

3.2: 3 h / 80 °C

3.3: 5 °C / pH 2.5

4.1: ethanol / 5 h / 80 °C

With sulfuric acid; hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.1016/j.ejmech.2012.04.024

Reference yield:

: 428508-13-8
2-(4-(methylsulfonyl)phenyl)acetohydrazide

: 1394240-77-7
6-(2,4-dichlorophenyl)-3-[4-(methylsulfonyl)benzyl]-7H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 10 h / 20 °C

1.2: 3 h / 80 °C

1.3: 5 °C / pH 2.5

2.1: ethanol / 5 h / 80 °C

With potassium hydroxide; In ethanol;
DOI:10.1016/j.ejmech.2012.04.024