N-[{(4S,5R)-2,2-dimethyl-5-[(methylsulfanyl)(diphenyl)methyl]-1,3-dioxolan-4-yl}(diphenyl)methyl]-1,1,1-trifluoromethanesulfonamide

Base Information

Chemical Name:N-[{(4S,5R)-2,2-dimethyl-5-[(methylsulfanyl)(diphenyl)methyl]-1,3-dioxolan-4-yl}(diphenyl)methyl]-1,1,1-trifluoromethanesulfonamide
CAS No.:1400792-83-7
Molecular Formula:C₃₃H₃₂F₃NO₄S₂
Molecular Weight:627.749
Hs Code.:

Synonyms:N-[{(4S,5R)-2,2-dimethyl-5-[(methylsulfanyl)(diphenyl)methyl]-1,3-dioxolan-4-yl}(diphenyl)methyl]-1,1,1-trifluoromethanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[{(4S,5R)-2,2-dimethyl-5-[(methylsulfanyl)(diphenyl)methyl]-1,3-dioxolan-4-yl}(diphenyl)methyl]-1,1,1-trifluoromethanesulfonamide

Chemical Property:

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Technology Process of N-[{(4S,5R)-2,2-dimethyl-5-[(methylsulfanyl)(diphenyl)methyl]-1,3-dioxolan-4-yl}(diphenyl)methyl]-1,1,1-trifluoromethanesulfonamide

There total 5 articles about N-[{(4S,5R)-2,2-dimethyl-5-[(methylsulfanyl)(diphenyl)methyl]-1,3-dioxolan-4-yl}(diphenyl)methyl]-1,1,1-trifluoromethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1400792-80-4
N-[{(4S,5R)-5-[(diphenyl)(sulfanyl)methyl]-2,2-dimethyl-1,3-dioxolan-4-yl}(diphenyl)methyl]-1,1,1-trifluoromethanesulfonamide

: 74-88-4
methyl iodide

: 1400792-83-7
N-[{(4S,5R)-2,2-dimethyl-5-[(methylsulfanyl)(diphenyl)methyl]-1,3-dioxolan-4-yl}(diphenyl)methyl]-1,1,1-trifluoromethanesulfonamide

Guidance literature:: With potassium carbonate; In dichloromethane; acetonitrile; at -10 - 20 ℃; for 7h;
DOI:10.1002/hlca.201200146

Reference yield:

: 1400792-74-6
N-({(4S,5R)-5-[(chloro)(diphenyl)methyl]-2,2-dimethyl-1,3-dioxolan-4-yl}diphenylmethyl)-1,1,1-trifluoromethanesulfonamide

: 1400792-83-7
N-[{(4S,5R)-2,2-dimethyl-5-[(methylsulfanyl)(diphenyl)methyl]-1,3-dioxolan-4-yl}(diphenyl)methyl]-1,1,1-trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: thiourea / dichloromethane; N,N-dimethyl-formamide / 72 h / 20 °C

1.2: 1 h

2.1: potassium carbonate / dichloromethane; acetonitrile / 7 h / -10 - 20 °C

With potassium carbonate; thiourea; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/hlca.201200146

Reference yield:

: 193892-87-4
N-{[(4S,5R)-5-(Diphenyl-trimethylsilanyloxy-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl}-C,C,C-trifluoro-methanesulfonamide

: 1400792-83-7
N-[{(4S,5R)-2,2-dimethyl-5-[(methylsulfanyl)(diphenyl)methyl]-1,3-dioxolan-4-yl}(diphenyl)methyl]-1,1,1-trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

2.1: thionyl chloride; lithium chloride / tetrahydrofuran / 6 h / Reflux

3.1: thiourea / dichloromethane; N,N-dimethyl-formamide / 72 h / 20 °C

3.2: 1 h

4.1: potassium carbonate / dichloromethane; acetonitrile / 7 h / -10 - 20 °C

With thionyl chloride; tetrabutyl ammonium fluoride; potassium carbonate; thiourea; lithium chloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/hlca.201200146