(1Z,2S,3S,4R,5R,6R,7R)-1-ethylidene-5,7-dihydroxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate

Base Information

• Chemical Name: (1Z,2S,3S,4R,5R,6R,7R)-1-ethylidene-5,7-dihydroxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate
• CAS No.: 1313587-26-6
• Molecular Formula: C₂₅H₄₀O₅
• Molecular Weight: 420.59

Synonyms:(1Z,2S,3S,4R,5R,6R,7R)-1-ethylidene-5,7-dihydroxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate

Chemical Property of (1Z,2S,3S,4R,5R,6R,7R)-1-ethylidene-5,7-dihydroxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of (1Z,2S,3S,4R,5R,6R,7R)-1-ethylidene-5,7-dihydroxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate

There total 2 articles about (1Z,2S,3S,4R,5R,6R,7R)-1-ethylidene-5,7-dihydroxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(1Z,2S,3R,4S,6R,7R)-1-ethylidene-7-hydroxy-2,4,6-trimethyl-5-oxo-3-[(1S)-1-phenylethoxy]octyl isobutyrate (1313587-25-5) → (1Z,2S,3S,4R,5R,6R,7R)-1-ethylidene-5,7-dihydroxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate (1313587-26-6)

Guidance literature:

With sodium tetrahydroborate; diethyl methoxy borane; In methanol; at -78 ℃; Inert atmosphere;

DOI:10.1002/ejoc.201100196

Reference yield:

C37H59BO5 → (1Z,2S,3S,4R,5R,6R,7R)-1-ethylidene-5,7-dihydroxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate (1313587-26-6)

Guidance literature:

C₃₇H₅₉BO₅; With sodium tetrahydroborate; In methanol; diethyl ether; hexane; at -78 ℃; for 5h; Inert atmosphere;

With dihydrogen peroxide; Rochelle's salt; In methanol; diethyl ether; hexane; water; at -5 ℃; for 14h; Inert atmosphere;

DOI:10.1002/ejoc.201100196

Reference yield: 89.0%

(1Z,2S,3S,4R,5R,6R,7R)-1-ethylidene-5,7-dihydroxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate (1313587-26-6) + 2,2-dimethoxy-propane (77-76-9) → (1Z,2S,3S,4S,5R,6R,7R)-1-ethylidene-5,7-isopropylidenedioxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate (1313587-27-7)

Guidance literature:

With toluene-4-sulfonic acid; at 5 - 20 ℃; Inert atmosphere;

DOI:10.1002/ejoc.201100196

upstream raw materials:

(1Z,2S,3R,4S,6R,7R)-1-ethylidene-7-hydroxy-2,4,6-trimethyl-5-oxo-3-[(1S)-1-phenylethoxy]octyl isobutyrate

Downstream raw materials:

(+)-(2R,3S,4S,6S,7S,8S,9R,10R,11R)-3-hydroxy-1,1:9,11-bis(isopropylidenedioxy)-4,6,8,10-tetramethyl-7-[(1S)-1-phenylethoxy]dodecan-5-one

(1Z,2S,3S,4S,5R,6R,7R)-1-ethylidene-5,7-isopropylidenedioxy-2,4,6-trimethyl-3-[(1S)-1-phenylethoxy]octyl isobutyrate

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