p-methoxy-α-bromoisobutyranilide

Base Information

• Chemical Name: p-methoxy-α-bromoisobutyranilide
• CAS No.: 1970-56-5
• Molecular Formula: C₁₁H₁₄BrNO₂
• Molecular Weight: 272.142

Synonyms:p-methoxy-α-bromoisobutyranilide

Chemical Property of p-methoxy-α-bromoisobutyranilide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of p-methoxy-α-bromoisobutyranilide

There total 2 articles about p-methoxy-α-bromoisobutyranilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-bromoisobutyric acid bromide (20769-85-1) + 4-methoxy-aniline (104-94-9) → p-methoxy-α-bromoisobutyranilide (1970-56-5)

Guidance literature:

With potassium carbonate; In 1,2-dichloro-ethane; at 20 ℃; Sealed tube;

DOI:10.1039/c5ra14798k

Reference yield:

→ p-methoxy-α-bromoisobutyranilide (1970-56-5)

Guidance literature:

aus /BRN= 746128/ (II), /BRN= 471556/ in Bzl., NaOAc in W.;

DOI:10.1248/yakushi1947.89.1_88

Reference yield: 94.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + p-methoxy-α-bromoisobutyranilide (1970-56-5) → C19H21NO2

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate; In acetone; at 100 ℃; for 1.5h;

DOI:10.1039/c7ra07306b

upstream raw materials:

2-bromoisobutyric acid bromide

4-methoxy-aniline

Downstream raw materials:

3-(4-Methoxyphenyl)-5,5-dimethyl-2-dimethylaminooxazolidin-4-one

N-(4-methoxyphenyl)-2-methylacrylamide

N-(4-Methoxy-phenyl)-N-[1-(4-methoxy-phenylcarbamoyl)-1-methyl-ethyl]-2-methyl-acrylamide

p-methoxy-α-nitroisobutyranilide

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